(1S)-2-(4-nitrophenyl)-1-(2-phenyl-1,3-thiazol-4-yl)ethan-1-amine hydrobromide

Base Information

Chemical Name:(1S)-2-(4-nitrophenyl)-1-(2-phenyl-1,3-thiazol-4-yl)ethan-1-amine hydrobromide
CAS No.:960157-85-1
Molecular Formula:BrH*C₁₇H₁₅N₃O₂S
Molecular Weight:406.303
Hs Code.:

Synonyms:(1S)-2-(4-nitrophenyl)-1-(2-phenyl-1,3-thiazol-4-yl)ethan-1-amine hydrobromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S)-2-(4-nitrophenyl)-1-(2-phenyl-1,3-thiazol-4-yl)ethan-1-amine hydrobromide

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Technology Process of (1S)-2-(4-nitrophenyl)-1-(2-phenyl-1,3-thiazol-4-yl)ethan-1-amine hydrobromide

There total 3 articles about (1S)-2-(4-nitrophenyl)-1-(2-phenyl-1,3-thiazol-4-yl)ethan-1-amine hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 293291-20-0
(S)-tert-butyl 4-bromo-1-(4-nitrophenyl)-3-oxobutan-2-ylcarbamate

: 2227-79-4
benzenecarbothioamide

: 960157-85-1
(1S)-2-(4-nitrophenyl)-1-(2-phenyl-1,3-thiazol-4-yl)ethan-1-amine hydrobromide

Guidance literature:: In acetonitrile; for 24h; Reflux;

Reference yield:

: 33305-77-0
Boc-Phe(p-NO₂)-OH

: 960157-85-1
(1S)-2-(4-nitrophenyl)-1-(2-phenyl-1,3-thiazol-4-yl)ethan-1-amine hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; isobutyl chloroformate / tetrahydrofuran / 0.33 h / 0 °C

1.2: 3 h / 0 - 20 °C

2.1: hydrogen bromide / water; tetrahydrofuran / 1.5 h / 0 °C

3.1: acetonitrile / 24 h / Reflux

With hydrogen bromide; triethylamine; isobutyl chloroformate; In tetrahydrofuran; water; acetonitrile;

Reference yield:

: 127106-74-5
(S)-[3-diazo-1-(4-nitrobenzyl)-2-oxo-propyl]carbamic acid tert-butyl ester

: 960157-85-1
(1S)-2-(4-nitrophenyl)-1-(2-phenyl-1,3-thiazol-4-yl)ethan-1-amine hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide / water; tetrahydrofuran / 1.5 h / 0 °C

2: acetonitrile / 24 h / Reflux

With hydrogen bromide; In tetrahydrofuran; water; acetonitrile;