C₅₅H₉₀O₆Si₃

Base Information

Chemical Name:C₅₅H₉₀O₆Si₃
CAS No.:1207069-44-0
Molecular Formula:C₅₅H₉₀O₆Si₃
Molecular Weight:931.572
Hs Code.:

C<sub>55</sub>H<sub>90</sub>O<sub>6</sub>Si<sub>3</sub>

Synonyms:C₅₅H₉₀O₆Si₃

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Chemical Property of C₅₅H₉₀O₆Si₃

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Technology Process of C₅₅H₉₀O₆Si₃

There total 6 articles about C₅₅H₉₀O₆Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1207069-46-2
C₂₄H₄₀O₃Si

: 1207069-45-1
C₃₃H₅₄O₃Si₂

: 1207069-44-0
C₅₅H₉₀O₆Si₃

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In dichloromethane; at 35 ℃; for 21h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol902778y

Reference yield:

: 910046-59-2
tert-butyl-[(3S)-(4-methoxybenzyloxy)hex-5-enyloxy]diphenylsilane

: 1207069-44-0
C₅₅H₉₀O₆Si₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water / 20 °C

1.2: 20 °C

2.1: magnesium bromide diethyl etherate / dichloromethane / 0 °C

3.1: 2,6-dimethylpyridine / dichloromethane / 0 °C

4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 20 °C / pH 7 / aq. buffer

5.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 35 °C

With 2,6-dimethylpyridine; osmium(VIII) oxide; Hoveyda-Grubbs catalyst second generation; magnesium bromide diethyl etherate; 4-methylmorpholine N-oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/chem.201003135

Reference yield:

: 1207069-48-4
C₃₂H₄₂O₄Si

: 1207069-44-0
C₅₅H₉₀O₆Si₃

Guidance literature:: Multi-step reaction with 3 steps

1: 2,6-dimethylpyridine / dichloromethane / 0 °C

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 20 °C / pH 7 / aq. buffer

3: Hoveyda-Grubbs catalyst second generation / dichloromethane / 35 °C

With 2,6-dimethylpyridine; Hoveyda-Grubbs catalyst second generation; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water;
DOI:10.1002/chem.201003135