1H-Imidazole-4-acetonitrile,5-amino-alpha-imino-1-methyl-(9CI)

Base Information

• Chemical Name: 1H-Imidazole-4-acetonitrile,5-amino-alpha-imino-1-methyl-(9CI)
• CAS No.: 765943-20-2
• Molecular Formula: C6H7 N5
• Molecular Weight: 149.155
• Mol file: 765943-20-2.mol

Synonyms:1H-Imidazole-4-acetonitrile,5-amino-alpha-imino-1-methyl-(9CI)

Chemical Property of 1H-Imidazole-4-acetonitrile,5-amino-alpha-imino-1-methyl-(9CI)

Chemical Property:

• PSA: 91.48000
• LogP: 0.57468

Purity/Quality:

5-amino-a-imino-1-methyl-1H-Imidazole-4-acetonitrile 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Imidazole-4-acetonitrile,5-amino-alpha-imino-1-methyl-(9CI)

There total 1 articles about 1H-Imidazole-4-acetonitrile,5-amino-alpha-imino-1-methyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

Ethyl (Z)-N-(2-amino-1,2-dicyanovinyl)formimidate (358657-89-3) → [5-amino-1-methyl-1H-imidazol-4-yl](imino)acetonitrile (765943-20-2)

Guidance literature:

Ethyl (Z)-N-(2-amino-1,2-dicyanovinyl)formimidate; With methylamine; In ethanol; at 20 ℃; for 5h;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In ethanol; at 20 ℃; Further stages.;

DOI:10.1002/ejoc.200700416

Reference yield: 96.0%

[5-amino-1-methyl-1H-imidazol-4-yl](imino)acetonitrile (765943-20-2) + 4-fluoroaniline (371-40-4) → C11H12FN5 (1354414-12-2)

Guidance literature:

With acetic acid; In acetonitrile; at 40 ℃; for 8h;

DOI:10.1055/s-0031-1289528

Reference yield: 79.0%

[5-amino-1-methyl-1H-imidazol-4-yl](imino)acetonitrile (765943-20-2) + Tosyl isocyanate (4083-64-1) → C14H14N6O3S + C14H14N6O3S

Guidance literature:

In acetonitrile; at -4 ℃; for 0.75h;

DOI:10.1002/ejoc.200601025

upstream raw materials:

Ethyl (Z)-N-(2-amino-1,2-dicyanovinyl)formimidate

Downstream raw materials:

C₁₄H₁₂N₆O₂

C₁₃H₁₁N₅O

C₁₄H₁₇N₅O

C₁₄H₁₅N₅