Technology Process of 2-(difluoroiodomethoxy)-1,1,2,2-tetrafluoroethanesulfonic acid phenyl ester
There total 1 articles about 2-(difluoroiodomethoxy)-1,1,2,2-tetrafluoroethanesulfonic acid phenyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
fluorosulfonyldifluoroacetyl fluoride;
With
potassium fluoride;
In
acetonitrile;
at 20 ℃;
for 2h;
difluorodiiodomethane;
In
acetonitrile;
at 45 ℃;
for 48h;
phenol;
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
dichloromethane;
at -60 - 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1016/j.jfluchem.2013.01.001