(S)-2-(3-Phenyl-2-propenoyl)-oxybutan-1,4-dicarbonsaeuredimethylester

Base Information

• Chemical Name: (S)-2-(3-Phenyl-2-propenoyl)-oxybutan-1,4-dicarbonsaeuredimethylester
• CAS No.: 124820-37-7
• Molecular Formula: C₁₅H₁₆O₆
• Molecular Weight: 292.288
• Mol file: 124820-37-7.mol

Synonyms:(S)-2-(3-Phenyl-2-propenoyl)-oxybutan-1,4-dicarbonsaeuredimethylester

Chemical Property of (S)-2-(3-Phenyl-2-propenoyl)-oxybutan-1,4-dicarbonsaeuredimethylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-2-(3-Phenyl-2-propenoyl)-oxybutan-1,4-dicarbonsaeuredimethylester

There total 3 articles about (S)-2-(3-Phenyl-2-propenoyl)-oxybutan-1,4-dicarbonsaeuredimethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

dimethyl (S)-malate (617-55-0) + (E)-3-phenylacrylic acid (140-10-3) → (S)-2-(3-Phenyl-2-propenoyl)-oxybutan-1,4-dicarbonsaeuredimethylester (124820-37-7)

Guidance literature:

With dicyclohexyl-carbodiimide; 4-pyrrolidin-1-ylpyridine; In dichloromethane; -10 to -5 deg C, 30 min then room temp.;

DOI:10.1002/ardp.19893220903

Reference yield:

Cinnamoyl chloride (102-92-1,17082-09-6) → (S)-2-(3-Phenyl-2-propenoyl)-oxybutan-1,4-dicarbonsaeuredimethylester (124820-37-7)

Guidance literature:

Multi-step reaction with 2 steps

2: hydrogen chloride

With hydrogenchloride;

Reference yield:

methanol (67-56-1) + O-trans-cinnamoyl-L-malic acid → (S)-2-(3-Phenyl-2-propenoyl)-oxybutan-1,4-dicarbonsaeuredimethylester (124820-37-7)

Guidance literature:

With hydrogenchloride;

upstream raw materials:

methanol

dimethyl (S)-malate

(E)-3-phenylacrylic acid

Cinnamoyl chloride