Technology Process of C32H37NP2
There total 4 articles about C32H37NP2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C20H27BrNP;
With
n-butyllithium;
In
diethyl ether;
at -35 - 20 ℃;
for 2h;
Schlenk technique;
Inert atmosphere;
chloro-diphenylphosphine;
In
diethyl ether;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/ic503062w
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / diethyl ether / 0.5 h / Cooling with acetone-dry ice
1.2: 12 h / Cooling with acetone-dry ice
2.1: n-butyllithium / diethyl ether / 2 h / -35 - 20 °C / Schlenk technique; Inert atmosphere
2.2: Inert atmosphere; Schlenk technique
With
n-butyllithium;
In
diethyl ether;
DOI:10.1021/ic503062w
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-Bromosuccinimide / dichloromethane / 48 h / 20 °C / Inert atmosphere
2.1: n-butyllithium / diethyl ether / 0.5 h / Cooling with acetone-dry ice
2.2: 12 h / Cooling with acetone-dry ice
3.1: n-butyllithium / diethyl ether / 2 h / -35 - 20 °C / Schlenk technique; Inert atmosphere
3.2: Inert atmosphere; Schlenk technique
With
N-Bromosuccinimide; n-butyllithium;
In
diethyl ether; dichloromethane;
DOI:10.1021/ic503062w