2'-(phenyl)ethyl 2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:2'-(phenyl)ethyl 2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-β-D-glucopyranoside
CAS No.:1202785-47-4
Molecular Formula:C₃₇H₄₁N₃O₆Si
Molecular Weight:651.835
Hs Code.:

Synonyms:2'-(phenyl)ethyl 2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-β-D-glucopyranoside

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Chemical Property of 2'-(phenyl)ethyl 2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-β-D-glucopyranoside

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Technology Process of 2'-(phenyl)ethyl 2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-β-D-glucopyranoside

There total 3 articles about 2'-(phenyl)ethyl 2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 659722-21-1
methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-glucopyranoside

: 60-12-8
2-phenylethanol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1202785-46-3
2'-(phenyl)ethyl 2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-α-D-glucopyranoside

: 1202785-47-4
2'-(phenyl)ethyl 2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-β-D-glucopyranoside

Guidance literature:: methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-glucopyranoside; 2-phenylethanol; In dichloromethane; for 1h; Molecular sieve; Inert atmosphere;

With dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In dichloromethane; at 20 ℃; Inert atmosphere;

tert-butylchlorodiphenylsilane; With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo9021919

Reference yield:

: C₃₇H₄₀N₃O₆PolSi

: 1202785-47-4
2'-(phenyl)ethyl 2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-β-D-glucopyranoside

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; solid phase reaction;
DOI:10.1021/jo9021919

Reference yield:

: 60-12-8
2-phenylethanol

: 1239364-99-8
bromo-2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-D-glucopyranoside

: 1202785-46-3
2'-(phenyl)ethyl 2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-α-D-glucopyranoside

: 1202785-47-4
2'-(phenyl)ethyl 2-azido-3-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 2.5h; optical yield given as %de; Molecular sieve; Inert atmosphere; Darkness;
DOI:10.1021/jm1002777