4-tert-Butyldimethylsilyloxy-2-methoxy-1-methoxymethoxy-6-pentylbenzene

Base Information

Chemical Name:4-tert-Butyldimethylsilyloxy-2-methoxy-1-methoxymethoxy-6-pentylbenzene
CAS No.:244770-97-6
Molecular Formula:C₂₀H₃₆O₄Si
Molecular Weight:368.589
Hs Code.:

Synonyms:4-tert-Butyldimethylsilyloxy-2-methoxy-1-methoxymethoxy-6-pentylbenzene

Suppliers and Price of 4-tert-Butyldimethylsilyloxy-2-methoxy-1-methoxymethoxy-6-pentylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-tert-Butyldimethylsilyloxy-2-methoxy-1-methoxymethoxy-6-pentylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-tert-Butyldimethylsilyloxy-2-methoxy-1-methoxymethoxy-6-pentylbenzene

There total 5 articles about 4-tert-Butyldimethylsilyloxy-2-methoxy-1-methoxymethoxy-6-pentylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5533-00-6
3-methoxy-4-methoxymethoxy-benzaldehyde

: 244770-97-6
4-tert-Butyldimethylsilyloxy-2-methoxy-1-methoxymethoxy-6-pentylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / m-CPBA / CH₂Cl₂ / 5 h / 25 °C

2: 78 percent / KOH, H₂O / ethanol / 0.17 h / 50 °C

3: 90 percent / imidazole / dimethylformamide / 7 h

With 1H-imidazole; potassium hydroxide; water; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-1999-3515

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 244770-97-6
4-tert-Butyldimethylsilyloxy-2-methoxy-1-methoxymethoxy-6-pentylbenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / NaH / dimethylformamide / 1.) 0 deg C, 15 min, 2.) 25 deg C, 14 h

2: 94 percent / m-CPBA / CH₂Cl₂ / 5 h / 25 °C

3: 78 percent / KOH, H₂O / ethanol / 0.17 h / 50 °C

4: 90 percent / imidazole / dimethylformamide / 7 h

With 1H-imidazole; potassium hydroxide; water; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-1999-3515

Reference yield:

: 104202-49-5
3-Methoxy-4-methoxymethoxyphenol

: 244770-97-6
4-tert-Butyldimethylsilyloxy-2-methoxy-1-methoxymethoxy-6-pentylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / imidazole / dimethylformamide / 7 h

With 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1055/s-1999-3515