4-tert-butyldiphenylsiloxy-1-(3,4-methylenedioxyphenyl)-2-phenylsulfonyl-1-butanone

Base Information

Chemical Name:4-tert-butyldiphenylsiloxy-1-(3,4-methylenedioxyphenyl)-2-phenylsulfonyl-1-butanone
CAS No.:171504-39-5
Molecular Formula:C₃₃H₃₄O₆SSi
Molecular Weight:586.781
Hs Code.:

Synonyms:4-tert-butyldiphenylsiloxy-1-(3,4-methylenedioxyphenyl)-2-phenylsulfonyl-1-butanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-tert-butyldiphenylsiloxy-1-(3,4-methylenedioxyphenyl)-2-phenylsulfonyl-1-butanone

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Technology Process of 4-tert-butyldiphenylsiloxy-1-(3,4-methylenedioxyphenyl)-2-phenylsulfonyl-1-butanone

There total 1 articles about 4-tert-butyldiphenylsiloxy-1-(3,4-methylenedioxyphenyl)-2-phenylsulfonyl-1-butanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 159598-70-6
4-tert-butyldiphenylsiloxy-1-(3,4-methylenedioxyphenyl)-2-phenylsulfonyl-1-butanol

: 171504-39-5
4-tert-butyldiphenylsiloxy-1-(3,4-methylenedioxyphenyl)-2-phenylsulfonyl-1-butanone

Guidance literature:: With 4 A molecular sieve; pyridinium chlorochromate; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1016/0040-4020(95)00565-P

Reference yield: 91.0%

: 75-36-5
acetyl chloride

: 171504-39-5
4-tert-butyldiphenylsiloxy-1-(3,4-methylenedioxyphenyl)-2-phenylsulfonyl-1-butanone

: (Z)-1-acetoxy-4-tert-butyldiphenylsiloxy-1-(3,4-methylenedioxyphenyl)-2-phenylsulfonyl-1-butene

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 0.333333h; Ambient temperature;
DOI:10.1016/0040-4020(95)00565-P

Reference yield:

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 171504-39-5
4-tert-butyldiphenylsiloxy-1-(3,4-methylenedioxyphenyl)-2-phenylsulfonyl-1-butanone

: (Z)-4-tert-butyldiphenylsiloxy-1-(diphenyloxyphosphinyl)oxy-1-(3,4-methylenedioxyphenyl)-2-phenylsulfonyl-1-butene

: (E)-4-tert-butyldiphenylsiloxy-1-(diphenyloxyphosphinyl)oxy-1-(3,4-methylenedioxyphenyl)-2-phenylsulfonyl-1-butene

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride; In tetrahydrofuran; for 0.333333h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1016/0040-4020(95)00565-P