butyl (benzoyl)phenyl phosphinate

Base Information

Chemical Name:butyl (benzoyl)phenyl phosphinate
CAS No.:18788-25-5
Molecular Formula:C₁₇H₁₉O₃P
Molecular Weight:302.31
Hs Code.:

Synonyms:butyl (benzoyl)phenyl phosphinate

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Chemical Property of butyl (benzoyl)phenyl phosphinate

Chemical Property:

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Technology Process of butyl (benzoyl)phenyl phosphinate

There total 4 articles about butyl (benzoyl)phenyl phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112298-91-6
butyl phenyl(phenylmethanol) phosphinate

: 18788-25-5
butyl (benzoyl)phenyl phosphinate

Guidance literature:: butyl phenyl(phenylmethanol) phosphinate; With N-chloro-succinimide; dimethylsulfide; In dichloromethane; at -78 ℃; for 1.33333h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - 20 ℃; for 1.25h; Inert atmosphere;
DOI:10.1021/ol3013793

Reference yield:

: 1382936-86-8
butyl (hydroxymethyl)phenyl phosphinate

: 18788-25-5
butyl (benzoyl)phenyl phosphinate

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-chloro-succinimide; dimethylsulfide / dichloromethane / 1.33 h / -78 °C / Inert atmosphere

1.2: 1.25 h / -78 - 20 °C / Inert atmosphere

2.1: triethylamine / toluene / 24 h / Reflux

3.1: N-chloro-succinimide; dimethylsulfide / dichloromethane / 1.33 h / -78 °C / Inert atmosphere

3.2: 1.25 h / -78 - 20 °C / Inert atmosphere

With N-chloro-succinimide; dimethylsulfide; triethylamine; In dichloromethane; toluene; 1.1: Corey-Kim oxidation / 1.2: Corey-Kim oxidation / 3.1: Corey-Kim oxidation / 3.2: Corey-Kim oxidation;
DOI:10.1021/ol3013793

Reference yield:

: 1779-48-2
phenylphosphinic acid

: 18788-25-5
butyl (benzoyl)phenyl phosphinate

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 24 h / Reflux; Inert atmosphere

2.1: triethylamine / toluene / 24 h / Reflux

3.1: N-chloro-succinimide; dimethylsulfide / dichloromethane / 1.33 h / -78 °C / Inert atmosphere

3.2: 1.25 h / -78 - 20 °C / Inert atmosphere

With N-chloro-succinimide; dimethylsulfide; triethylamine; In dichloromethane; toluene; 3.1: Corey-Kim oxidation / 3.2: Corey-Kim oxidation;
DOI:10.1021/ol3013793