butyl phenyl(phenylmethanol) phosphinate

Base Information

Chemical Name:butyl phenyl(phenylmethanol) phosphinate
CAS No.:112298-91-6
Molecular Formula:C₁₇H₂₁O₃P
Molecular Weight:304.326
Hs Code.:

Synonyms:butyl phenyl(phenylmethanol) phosphinate

Suppliers and Price of butyl phenyl(phenylmethanol) phosphinate

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Chemical Property of butyl phenyl(phenylmethanol) phosphinate

Chemical Property:

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Technology Process of butyl phenyl(phenylmethanol) phosphinate

There total 3 articles about butyl phenyl(phenylmethanol) phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6172-81-2
butyl phenylphosphinate

: 100-52-7
benzaldehyde

: 112298-91-6
butyl phenyl(phenylmethanol) phosphinate

Guidance literature:

Reference yield:

: 1382936-86-8
butyl (hydroxymethyl)phenyl phosphinate

: 112298-91-6
butyl phenyl(phenylmethanol) phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-chloro-succinimide; dimethylsulfide / dichloromethane / 1.33 h / -78 °C / Inert atmosphere

1.2: 1.25 h / -78 - 20 °C / Inert atmosphere

2.1: triethylamine / toluene / 24 h / Reflux

With N-chloro-succinimide; dimethylsulfide; triethylamine; In dichloromethane; toluene; 1.1: Corey-Kim oxidation / 1.2: Corey-Kim oxidation;
DOI:10.1021/ol3013793

Reference yield:

: 1779-48-2
phenylphosphinic acid

: 112298-91-6
butyl phenyl(phenylmethanol) phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 24 h / Reflux; Inert atmosphere

2: triethylamine / toluene / 24 h / Reflux

With triethylamine; In toluene;
DOI:10.1021/ol3013793