biphenyl-4-yl[4-(3,4-dimethoxyphenyl)-6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl]methanone

Base Information

Chemical Name:biphenyl-4-yl[4-(3,4-dimethoxyphenyl)-6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl]methanone
CAS No.:1427266-36-1
Molecular Formula:C₃₂H₃₁NO₅
Molecular Weight:509.602
Hs Code.:

Synonyms:biphenyl-4-yl[4-(3,4-dimethoxyphenyl)-6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl]methanone

Suppliers and Price of biphenyl-4-yl[4-(3,4-dimethoxyphenyl)-6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl]methanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of biphenyl-4-yl[4-(3,4-dimethoxyphenyl)-6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl]methanone

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Technology Process of biphenyl-4-yl[4-(3,4-dimethoxyphenyl)-6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl]methanone

There total 2 articles about biphenyl-4-yl[4-(3,4-dimethoxyphenyl)-6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl]methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1427266-31-6
N-(2,2-bis(3,4-dimethoxyphenyl)ethyl)-[1,1'-biphenyl]-4-carboxamide

: 1427266-36-1
biphenyl-4-yl[4-(3,4-dimethoxyphenyl)-6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl]methanone

Guidance literature:: With silica gel; In 1,2-dichloro-ethane; at 80 ℃; for 1h;
DOI:10.3390/molecules18021869

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 1427266-36-1
biphenyl-4-yl[4-(3,4-dimethoxyphenyl)-6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl]methanone

Guidance literature:: Multi-step reaction with 3 steps

1: polyphosphoric acid / 0.33 h / 20 °C

2: triethylamine / dichloromethane / 0.67 h / 20 °C

3: silica gel / 1,2-dichloro-ethane / 1 h / 80 °C

With silica gel; triethylamine; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.3390/molecules18021869