(1R,αR)-N-(1-phenylethyl)cyclohexanamine

Base Information

Chemical Name:(1R,αR)-N-(1-phenylethyl)cyclohexanamine
CAS No.:147021-76-9
Molecular Formula:C₁₄H₂₁N
Molecular Weight:203.327
Hs Code.:

Synonyms:(1R,αR)-N-(1-phenylethyl)cyclohexanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,αR)-N-(1-phenylethyl)cyclohexanamine

Chemical Property:

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Technology Process of (1R,αR)-N-(1-phenylethyl)cyclohexanamine

There total 11 articles about (1R,αR)-N-(1-phenylethyl)cyclohexanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 147021-76-9
(1R,αR)-N-(1-phenylethyl)cyclohexanamine

Guidance literature:: Multi-step reaction with 3 steps

1: chiral rhodium(I) complex / tetrahydrofuran / 1 h / 20 °C

2: toluene / 2 h

3: toluene; diethyl ether / 1.08 h / 0 - 20 °C

chiral rhodium(I); In tetrahydrofuran; diethyl ether; toluene; 1: Addition / 2: Substitution / 3: Alkylation;

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 147021-76-9
(1R,αR)-N-(1-phenylethyl)cyclohexanamine

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOCl / diethyl ether / 0 °C

2: toluene; diethyl ether / 1.08 h / 0 - 20 °C

With sodium hypochlorite; In diethyl ether; toluene; 1: Chlorination / 2: Alkylation;

Reference yield:

: 731797-80-1
N-(1-phenylethylidene)cycloexanamine

: 66399-53-9
(1S,αS)-N-(1-phenylethyl)cyclohexanamine

: 147021-76-9
(1R,αR)-N-(1-phenylethyl)cyclohexanamine

Guidance literature:: With C₂₁H₃₄BN₂O₂⁽¹⁺⁾*C₂F₆NO₄S₂^(1-); hydrogen; at 30 ℃; for 16h; under 75757.6 Torr; Overall yield = 67 %; enantioselective reaction; Glovebox; Sealed tube;
DOI:10.1039/c9cc02900a