N-(1-phenylethylidene)cycloexanamine

Base Information

• Chemical Name: N-(1-phenylethylidene)cycloexanamine
• CAS No.: 731797-80-1
• Molecular Formula: C₁₄H₁₉N
• Molecular Weight: 201.312

Synonyms:N-(1-phenylethylidene)cycloexanamine

Chemical Property of N-(1-phenylethylidene)cycloexanamine

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Technology Process of N-(1-phenylethylidene)cycloexanamine

There total 2 articles about N-(1-phenylethylidene)cycloexanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

cyclohexylamine (108-91-8,157973-60-9) + acetophenone (98-86-2) → N-(1-phenylethylidene)cycloexanamine (731797-80-1)

Guidance literature:

With titanium tetrachloride; at 20 ℃; for 1.5h;

DOI:10.1039/c9cc02900a

Reference yield:

cyclohexylamine (108-91-8,157973-60-9) + phenylacetylene (536-74-3) → N-(1-phenylethylidene)cycloexanamine (731797-80-1) + Cyclohexyl-[2-phenyl-eth-(E)-ylidene]-amine

Guidance literature:

Ti(NMe₂)2(dpma); at 75 ℃; for 20h;

DOI:10.1039/b415701j

Reference yield: 86.0%

methacryloyl isocyanate (4474-60-6) + N-(1-phenylethylidene)cycloexanamine (731797-80-1) → 6-Cyclohexylamino-2-isopropenyl-6-phenyl-6H-[1,3]oxazin-4-ol (184531-34-8)

Guidance literature:

In benzene; for 1h; Heating;

upstream raw materials:

cyclohexylamine

phenylacetylene

acetophenone

Downstream raw materials:

1-phenylpentane-1,4-dione

6-Cyclohexylamino-2-isopropenyl-6-phenyl-6H-[1,3]oxazin-4-ol

(Z)-3-cyclohexylamino-1-(1H-1-imidazolyl)-3-phenyl-2-propen-1-one

N-(1-phenylethyl)cyclohexanamine

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