CH₃O-Adip-Lys(Z)-OBu-t

Base Information

Chemical Name:CH₃O-Adip-Lys(Z)-OBu-t
CAS No.:93489-31-7
Molecular Formula:C₂₅H₃₈N₂O₇
Molecular Weight:478.586
Hs Code.:

Synonyms:CH₃O-Adip-Lys(Z)-OBu-t

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Chemical Property of CH₃O-Adip-Lys(Z)-OBu-t

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Technology Process of CH₃O-Adip-Lys(Z)-OBu-t

There total 1 articles about CH₃O-Adip-Lys(Z)-OBu-t which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 627-91-8
adipic acid monomethyl ester

: 5978-22-3,1426213-63-9
N(ε)-benzoyloxycarbonyl-L-lysine tert-butyl ester hydrochloride

: 93489-31-7
CH₃O-Adip-Lys(Z)-OBu-t

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; 1 h, 0 deg C => 6 h, r.t.;

Reference yield:

: 93489-31-7
CH₃O-Adip-Lys(Z)-OBu-t

: 93511-73-0
CH3O-Adip-Lys(εAhx-Nps)-OBu-t

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / H₂ / Pd/C / methanol; acetic acid / 4 h / Ambient temperature

2: 99 percent / 1-hydroxybenzotriazole, N-ethyl-N'-(3-dimethylaminopropyl)-carbodiimide HCl / tetrahydrofuran; various solvent(s) / 2 h, 0 deg C => 2 h, r.t.

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In tetrahydrofuran; methanol; acetic acid;

Reference yield:

: 93489-31-7
CH₃O-Adip-Lys(Z)-OBu-t

: 93489-36-2
SuNO-Adip-Lys(εAhx-Nps)-OBu-t

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / H₂ / Pd/C / methanol; acetic acid / 4 h / Ambient temperature

2: 99 percent / 1-hydroxybenzotriazole, N-ethyl-N'-(3-dimethylaminopropyl)-carbodiimide HCl / tetrahydrofuran; various solvent(s) / 2 h, 0 deg C => 2 h, r.t.

3: 88 percent / NaOH (1 M) / dioxane; H₂O / 1 h / Ambient temperature

4: 71 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 2 h, 0 deg C => 2 h, r.t.

With sodium hydroxide; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; water; acetic acid;