5-(benzyloxy)-1-methyl-1-<3-(2-methyl-1,3-dioxolan-2-yl)propyl>pent-2-ynyl benzoate

Base Information

Chemical Name:5-(benzyloxy)-1-methyl-1-<3-(2-methyl-1,3-dioxolan-2-yl)propyl>pent-2-ynyl benzoate
CAS No.:222613-39-0
Molecular Formula:C₂₇H₃₂O₅
Molecular Weight:436.548
Hs Code.:

Synonyms:5-(benzyloxy)-1-methyl-1-<3-(2-methyl-1,3-dioxolan-2-yl)propyl>pent-2-ynyl benzoate

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Chemical Property of 5-(benzyloxy)-1-methyl-1-<3-(2-methyl-1,3-dioxolan-2-yl)propyl>pent-2-ynyl benzoate

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Technology Process of 5-(benzyloxy)-1-methyl-1-<3-(2-methyl-1,3-dioxolan-2-yl)propyl>pent-2-ynyl benzoate

There total 3 articles about 5-(benzyloxy)-1-methyl-1-<3-(2-methyl-1,3-dioxolan-2-yl)propyl>pent-2-ynyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53750-51-9
2-methyl-2-(2-iodoethyl)-1,3-dioxolane

: 222613-39-0
5-(benzyloxy)-1-methyl-1-<3-(2-methyl-1,3-dioxolan-2-yl)propyl>pent-2-ynyl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: LDA / tetrahydrofuran / 0 - 20 °C

2: aq. HCl / tetrahydrofuran / 2 h / 0 °C

3: 1.) BuLi

With hydrogenchloride; n-butyllithium; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/jo9819133

Reference yield:

: 90719-11-2
N,N-dimethyl-N'-[1-methyl-4-(2-methyl-[1,3]dioxolan-2-yl)-butylidene]-hydrazine

: 222613-39-0
5-(benzyloxy)-1-methyl-1-<3-(2-methyl-1,3-dioxolan-2-yl)propyl>pent-2-ynyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl / tetrahydrofuran / 2 h / 0 °C

2: 1.) BuLi

With hydrogenchloride; n-butyllithium; In tetrahydrofuran;
DOI:10.1021/jo9819133