N,N,N-tris<8-(tetrahydro-2H-pyran-2-yl)oxy-3-tosyl-6-oxa-3-azaoctyl>amine

Base Information

Chemical Name:N,N,N-tris<8-(tetrahydro-2H-pyran-2-yl)oxy-3-tosyl-6-oxa-3-azaoctyl>amine
CAS No.:98846-93-6
Molecular Formula:C₅₄H₈₄N₄O₁₅S₃
Molecular Weight:1125.48
Hs Code.:

Synonyms:N,N,N-tris<8-(tetrahydro-2H-pyran-2-yl)oxy-3-tosyl-6-oxa-3-azaoctyl>amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N,N-tris<8-(tetrahydro-2H-pyran-2-yl)oxy-3-tosyl-6-oxa-3-azaoctyl>amine

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Technology Process of N,N,N-tris<8-(tetrahydro-2H-pyran-2-yl)oxy-3-tosyl-6-oxa-3-azaoctyl>amine

There total 7 articles about N,N,N-tris<8-(tetrahydro-2H-pyran-2-yl)oxy-3-tosyl-6-oxa-3-azaoctyl>amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 54533-84-5
2-(2-(2-chloroethoxy)ethoxy)tetrahydro-2H-pyran

: 98846-92-5
tris[2-(N-tosylaminoethyl)]amine

: 98846-93-6
N,N,N-tris<8-(tetrahydro-2H-pyran-2-yl)oxy-3-tosyl-6-oxa-3-azaoctyl>amine

Guidance literature:: With sodium; potassium carbonate; In methanol; N,N-dimethyl-formamide; at 110 ℃; for 8h;
DOI:10.1002/hlca.19850680202

Reference yield:

: 4097-89-6
2,2',2''-triaminotriethylamine

: 98846-93-6
N,N,N-tris<8-(tetrahydro-2H-pyran-2-yl)oxy-3-tosyl-6-oxa-3-azaoctyl>amine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / NaOH / H₂O; diethyl ether / 14 h / Ambient temperature

2: 1.) NaH; 2.) K₂CO₃ / 1.) DMF, r.t., 1.5 h; 2.) 100 degC, DMF, 19 h

With sodium hydroxide; sodium hydride; potassium carbonate; In diethyl ether; water;
DOI:10.1016/0040-4020(94)00965-W

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 98846-93-6
N,N,N-tris<8-(tetrahydro-2H-pyran-2-yl)oxy-3-tosyl-6-oxa-3-azaoctyl>amine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / NaOH / H₂O; diethyl ether / 14 h / Ambient temperature

2: 1.) NaH; 2.) K₂CO₃ / 1.) DMF, r.t., 1.5 h; 2.) 100 degC, DMF, 19 h

With sodium hydroxide; sodium hydride; potassium carbonate; In diethyl ether; water;
DOI:10.1016/0040-4020(94)00965-W