allyl 3-O-(2-O-benzyl-α-L-fucopyranosyl)-2-O-benzyl-α-L-fucopyranoside

Base Information

Chemical Name:allyl 3-O-(2-O-benzyl-α-L-fucopyranosyl)-2-O-benzyl-α-L-fucopyranoside
CAS No.:488719-74-0
Molecular Formula:C₂₉H₃₈O₉
Molecular Weight:530.615
Hs Code.:

Synonyms:allyl 3-O-(2-O-benzyl-α-L-fucopyranosyl)-2-O-benzyl-α-L-fucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 3-O-(2-O-benzyl-α-L-fucopyranosyl)-2-O-benzyl-α-L-fucopyranoside

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Technology Process of allyl 3-O-(2-O-benzyl-α-L-fucopyranosyl)-2-O-benzyl-α-L-fucopyranoside

There total 2 articles about allyl 3-O-(2-O-benzyl-α-L-fucopyranosyl)-2-O-benzyl-α-L-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₄₃H₄₅O₁₄S^(1-)*Na⁽¹⁺⁾

: 488719-74-0
allyl 3-O-(2-O-benzyl-α-L-fucopyranosyl)-2-O-benzyl-α-L-fucopyranoside

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 1h;
DOI:10.1081/CAR-120013500

Reference yield:

: 2-O-benzyl-3,4-di-O-chloroacetyl-L-fucopyranosyl trichloroacetimidate

: 327593-88-4
allyl 2-O-benzyl-α-L-fucopyranoside

: 488719-74-0
allyl 3-O-(2-O-benzyl-α-L-fucopyranosyl)-2-O-benzyl-α-L-fucopyranoside

Guidance literature:: 2-O-benzyl-3,4-di-O-chloroacetyl-L-fucopyranosyl trichloroacetimidate; allyl 2-O-benzyl-α-L-fucopyranoside; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere; Molecular sieve;

With trimethyl((trifluoromethyl)sulfonyl)silane; In dichloromethane; at -30 ℃; for 0.25h; Inert atmosphere;
DOI:10.3390/md13020770

Reference yield: 77.0%

: 98-88-4
benzoyl chloride

: 488719-74-0
allyl 3-O-(2-O-benzyl-α-L-fucopyranosyl)-2-O-benzyl-α-L-fucopyranoside

: 488719-75-1
allyl 3-O-(3-O-benzoyl-2-O-benzyl-α-L-fucopyranosyl)-2-O-benzyl-α-L-fucopyranoside

Guidance literature:: allyl 3-O-(2-O-benzyl-α-L-fucopyranosyl)-2-O-benzyl-α-L-fucopyranoside; With di(n-butyl)tin oxide; In toluene; Heating;

benzoyl chloride; In toluene; at 20 ℃; for 3h;
DOI:10.1081/CAR-120013500