2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxy-5-nitrophenyl)ethanonitrile

Base Information

Chemical Name:2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxy-5-nitrophenyl)ethanonitrile
CAS No.:114574-54-8
Molecular Formula:C₁₆H₂₄N₂O₅Si
Molecular Weight:352.462
Hs Code.:

Synonyms:2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxy-5-nitrophenyl)ethanonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxy-5-nitrophenyl)ethanonitrile

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Technology Process of 2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxy-5-nitrophenyl)ethanonitrile

There total 2 articles about 2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxy-5-nitrophenyl)ethanonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 22027-96-9
5-nitroveratral

: 151-50-8
potassium cyanide

: 18162-48-6
tert-butyldimethylsilyl chloride

: 114574-54-8
2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxy-5-nitrophenyl)ethanonitrile

Guidance literature:: With zinc(II) iodide; In acetonitrile; for 48h;
DOI:10.1016/S0040-4020(01)87665-1

Reference yield:

: 6635-20-7
isonitrovanillin

: 114574-54-8
2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxy-5-nitrophenyl)ethanonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / sodium hydroxyde, benzyltributylammonium bromide / CH₂Cl₂ / 24 h

2: 83 percent / zinc iodide / acetonitrile / 48 h

With sodium hydroxide; benzyl tri-n-butylammonium bromide; zinc(II) iodide; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)87665-1