{(vinyldiphenylphosphine)(μ-η3-diphenylphosphaallyl)palladium(I)}2(BF4)2

Base Information

Chemical Name:{(vinyldiphenylphosphine)(μ-η3-diphenylphosphaallyl)palladium(I)}2(BF4)2
CAS No.:126217-52-5
Molecular Formula:2BF₄*C₅₆H₅₂P₄Pd₂
Molecular Weight:1235.37
Hs Code.:

Synonyms:{(vinyldiphenylphosphine)(μ-η3-diphenylphosphaallyl)palladium(I)}2(BF4)2

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Chemical Property of {(vinyldiphenylphosphine)(μ-η3-diphenylphosphaallyl)palladium(I)}2(BF4)2

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Technology Process of {(vinyldiphenylphosphine)(μ-η3-diphenylphosphaallyl)palladium(I)}2(BF4)2

There total 1 articles about {(vinyldiphenylphosphine)(μ-η3-diphenylphosphaallyl)palladium(I)}2(BF4)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 14104-20-2
silver tetrafluoroborate

: 78629-73-9,113214-83-8,98717-39-6
{Pd(II)Cl₂(diphenylvinylphosphine)2}

: 126217-52-5
{(vinyldiphenylphosphine)(μ-η3-diphenylphosphaallyl)palladium(I)}2(BF4)2

Guidance literature:: In dichloromethane; byproducts: silver chloride, BF3; (N2); addn. of 2 equiv. of AgBF4 to Pd-compd. dissolved in CH2Cl2, pptn. of AgCl, stirring mixt. under ambient light (1 week); filtration, evapn., recrystn. by diffusion of Et2O into soln. of product in CH2Cl2/Et2O 3:1 at -20°C; elem. anal.;

Reference yield: 87.8%

: 126217-52-5
{(vinyldiphenylphosphine)(μ-η3-diphenylphosphaallyl)palladium(I)}2(BF4)2

: sym-trans-bis(μ-iodo)bis{iodo(diphenylvinylphosphine)palladium(II)}

Guidance literature:: With I₂; In dichloromethane; byproducts: CH2CHPO(C6H5)2, HI, HBF4; to a soln. of the complex in CH2Cl2 was added I2 under N2, stirred for 4 h at room temp.; vol. was reduced, addn. of Et2O, filtn., washed with Et2O, recrystd. from CH2Cl2/Et2O; elem. anal.;