2-allylmercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine

Base Information

• Chemical Name: 2-allylmercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine
• CAS No.: 123971-77-7
• Molecular Formula: C₁₉H₁₈N₂OS₂
• Molecular Weight: 354.497

Synonyms:2-allylmercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine

Chemical Property of 2-allylmercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine

Chemical Property:

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Technology Process of 2-allylmercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine

There total 6 articles about 2-allylmercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-mercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine sodium salt (101515-73-5) + 3-chloroprop-1-ene (107-05-1) → 2-allylmercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine (123971-77-7)

Guidance literature:

In ethanol; for 1h; Heating;

DOI:10.1007/BF00472400

Reference yield: 58.0%

3-phenyl-2-thio-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine (42076-13-1) → 2-allylmercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine (123971-77-7)

Guidance literature:

With potassium hydroxide; In ethanol;

DOI:10.1016/j.bmcl.2006.11.056

Reference yield: 58.0%

→ 2-allylmercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine (123971-77-7)

Guidance literature:

upstream raw materials:

2-mercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine sodium salt

3-chloroprop-1-ene

3-phenyl-2-thio-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine

ethyl 2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate

Downstream raw materials:

<2-(3-phenyl-2',4'-dioxo-5',6',7',8'-tetrahydrobenzothieno<2,3-d>-1'-pyrimidyl)propen-3-yl> disulfide

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