N-tert-butyl-N'-[1,1-bis(4-methylphenyl)-1-(methoxycarbonyl)methyl]sulfamide

Base Information

Chemical Name:N-tert-butyl-N'-[1,1-bis(4-methylphenyl)-1-(methoxycarbonyl)methyl]sulfamide
CAS No.:309253-27-8
Molecular Formula:C₂₁H₂₈N₂O₄S
Molecular Weight:404.53
Hs Code.:

Synonyms:N-tert-butyl-N'-[1,1-bis(4-methylphenyl)-1-(methoxycarbonyl)methyl]sulfamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-tert-butyl-N'-[1,1-bis(4-methylphenyl)-1-(methoxycarbonyl)methyl]sulfamide

Chemical Property:

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Technology Process of N-tert-butyl-N'-[1,1-bis(4-methylphenyl)-1-(methoxycarbonyl)methyl]sulfamide

There total 4 articles about N-tert-butyl-N'-[1,1-bis(4-methylphenyl)-1-(methoxycarbonyl)methyl]sulfamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 33581-95-2
tert-butylsulfamyl chloride

: 309253-14-3
amino-di-p-tolyl-acetic acid methyl ester

: 309253-27-8
N-tert-butyl-N'-[1,1-bis(4-methylphenyl)-1-(methoxycarbonyl)methyl]sulfamide

Guidance literature:: With triethylamine; In hexane; at -78 ℃; for 0.5h;
DOI:10.1002/jhet.5570370418

Reference yield:

: 611-97-2
bis(p-methylphenyl)-methanone

: 309253-27-8
N-tert-butyl-N'-[1,1-bis(4-methylphenyl)-1-(methoxycarbonyl)methyl]sulfamide

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / ammonium carbonate / various solvent(s) / Heating

2: 99 percent / aq. NaOH

3: 43 percent / HCl (g); Sodium sulfate

4: 86 percent / Et₃N / hexane / 0.5 h / -78 °C

With ammonium carbonate; hydrogenchloride; sodium hydroxide; sodium sulfate; triethylamine; In hexane; 1: modified Bucherer-Bergs reaction / 2: Hydrolysis / 3: Esterification / 4: Condensation;
DOI:10.1002/jhet.5570370418

Reference yield:

: 50373-76-7
5,5-bis(4-methylphenyl)imidazolidine-2,4-dione

: 309253-27-8
N-tert-butyl-N'-[1,1-bis(4-methylphenyl)-1-(methoxycarbonyl)methyl]sulfamide

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / aq. NaOH

2: 43 percent / HCl (g); Sodium sulfate

3: 86 percent / Et₃N / hexane / 0.5 h / -78 °C

With hydrogenchloride; sodium hydroxide; sodium sulfate; triethylamine; In hexane; 1: Hydrolysis / 2: Esterification / 3: Condensation;
DOI:10.1002/jhet.5570370418