N-{2-[1-(2-ethanesulfonylamino-phenyl)-cyclohexa-2,5-dienyl]ethyl}acetamide

Base Information

Chemical Name:N-{2-[1-(2-ethanesulfonylamino-phenyl)-cyclohexa-2,5-dienyl]ethyl}acetamide
CAS No.:955116-92-4
Molecular Formula:C₁₈H₂₄N₂O₃S
Molecular Weight:348.466
Hs Code.:

Synonyms:N-{2-[1-(2-ethanesulfonylamino-phenyl)-cyclohexa-2,5-dienyl]ethyl}acetamide

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Chemical Property of N-{2-[1-(2-ethanesulfonylamino-phenyl)-cyclohexa-2,5-dienyl]ethyl}acetamide

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Technology Process of N-{2-[1-(2-ethanesulfonylamino-phenyl)-cyclohexa-2,5-dienyl]ethyl}acetamide

There total 4 articles about N-{2-[1-(2-ethanesulfonylamino-phenyl)-cyclohexa-2,5-dienyl]ethyl}acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 955116-98-0
ethanesulfonic acid {2-[1-(2-aminoethyl)-cyclohexa-2,5-dienyl]phenyl}amide

: 108-24-7
acetic anhydride

: 955116-92-4
N-{2-[1-(2-ethanesulfonylamino-phenyl)-cyclohexa-2,5-dienyl]ethyl}acetamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/ol701493k

Reference yield:

: 57638-94-5
ethanesulfonic acid biphenyl-2-ylamide

: 955116-92-4
N-{2-[1-(2-ethanesulfonylamino-phenyl)-cyclohexa-2,5-dienyl]ethyl}acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -78 °C

1.2: Li; NH₃ / tetrahydrofuran; hexane / 0.5 h / -78 °C

1.3: 70 percent / tetrahydrofuran; hexane / 0.17 h / -78 °C

2.1: LiAlH₄; AlCl₃ / tetrahydrofuran / 4 h / 20 °C

3.1: 0.695 g / Et₃N / CH₂Cl₂ / 12 h / 20 °C

With lithium aluminium tetrahydride; n-butyllithium; aluminium trichloride; triethylamine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol701493k

Reference yield:

: 955116-90-2
ethanesulfonic acid [2-(1-cyanomethyl-cyclohexa-2,5-dienyl)phenyl]carbamic amide

: 955116-92-4
N-{2-[1-(2-ethanesulfonylamino-phenyl)-cyclohexa-2,5-dienyl]ethyl}acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄; AlCl₃ / tetrahydrofuran / 4 h / 20 °C

2: 0.695 g / Et₃N / CH₂Cl₂ / 12 h / 20 °C

With lithium aluminium tetrahydride; aluminium trichloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol701493k