ethanesulfonic acid {2-[1-(2-aminoethyl)-cyclohexa-2,5-dienyl]phenyl}amide

Base Information

Chemical Name:ethanesulfonic acid {2-[1-(2-aminoethyl)-cyclohexa-2,5-dienyl]phenyl}amide
CAS No.:955116-98-0
Molecular Formula:C₁₆H₂₂N₂O₂S
Molecular Weight:306.429
Hs Code.:

Synonyms:ethanesulfonic acid {2-[1-(2-aminoethyl)-cyclohexa-2,5-dienyl]phenyl}amide

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Chemical Property of ethanesulfonic acid {2-[1-(2-aminoethyl)-cyclohexa-2,5-dienyl]phenyl}amide

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Technology Process of ethanesulfonic acid {2-[1-(2-aminoethyl)-cyclohexa-2,5-dienyl]phenyl}amide

There total 4 articles about ethanesulfonic acid {2-[1-(2-aminoethyl)-cyclohexa-2,5-dienyl]phenyl}amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₁₈N₂O₂S

: 955116-98-0
ethanesulfonic acid {2-[1-(2-aminoethyl)-cyclohexa-2,5-dienyl]phenyl}amide

Guidance literature:: With aluminum (III) chloride; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 18h;
DOI:10.1016/j.tet.2018.12.043

Reference yield:

: 955116-90-2
ethanesulfonic acid [2-(1-cyanomethyl-cyclohexa-2,5-dienyl)phenyl]carbamic amide

: 955116-98-0
ethanesulfonic acid {2-[1-(2-aminoethyl)-cyclohexa-2,5-dienyl]phenyl}amide

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1021/ol701493k

Reference yield:

: 57638-94-5
ethanesulfonic acid biphenyl-2-ylamide

: 955116-98-0
ethanesulfonic acid {2-[1-(2-aminoethyl)-cyclohexa-2,5-dienyl]phenyl}amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -78 °C

1.2: Li; NH₃ / tetrahydrofuran; hexane / 0.5 h / -78 °C

1.3: 70 percent / tetrahydrofuran; hexane / 0.17 h / -78 °C

2.1: LiAlH₄; AlCl₃ / tetrahydrofuran / 4 h / 20 °C

With lithium aluminium tetrahydride; n-butyllithium; aluminium trichloride; In tetrahydrofuran; hexane;
DOI:10.1021/ol701493k