ethyl phenyl benzoylphosphonate

Base Information

• Chemical Name: ethyl phenyl benzoylphosphonate
• CAS No.: 118433-67-3
• Molecular Formula: C₁₅H₁₅O₄P
• Molecular Weight: 290.255
• Mol file: 118433-67-3.mol

Synonyms:ethyl phenyl benzoylphosphonate

Chemical Property of ethyl phenyl benzoylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of ethyl phenyl benzoylphosphonate

There total 1 articles about ethyl phenyl benzoylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

diethyl phenyl phosphite (4894-60-4) + benzoyl chloride (98-88-4) → ethyl phenyl benzoylphosphonate (118433-67-3)

Guidance literature:

at 50 ℃; for 0.5h;

DOI:10.1007/BF00766865

Reference yield: 55.0%

ethyl phenyl benzoylphosphonate (118433-67-3) → phenyl sodium benzoylphosphonate

Guidance literature:

With sodium iodide; In acetone; at 20 ℃; for 24h;

DOI:10.1039/b010152o

Reference yield:

ethyl phenyl benzoylphosphonate (118433-67-3) → phenyl sodium α-hydroxyiminobenzylphosphonate

Guidance literature:

Multi-step reaction with 2 steps

1: 55 percent / NaI / acetone / 24 h / 20 °C

2: 41 percent / NH₂OH / methanol / 72 h / 20 °C

With hydroxylamine; sodium iodide; In methanol; acetone;

DOI:10.1039/b010152o

upstream raw materials:

diethyl phenyl phosphite

benzoyl chloride