dimethyl 2-((2-nitrobenzyl)oxy)terephthalate

Base Information

Chemical Name:dimethyl 2-((2-nitrobenzyl)oxy)terephthalate
CAS No.:1264669-97-7
Molecular Formula:C₁₇H₁₅NO₇
Molecular Weight:345.309
Hs Code.:

Synonyms:dimethyl 2-((2-nitrobenzyl)oxy)terephthalate

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Chemical Property of dimethyl 2-((2-nitrobenzyl)oxy)terephthalate

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Technology Process of dimethyl 2-((2-nitrobenzyl)oxy)terephthalate

There total 3 articles about dimethyl 2-((2-nitrobenzyl)oxy)terephthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 6342-72-9
dimethyl hydroxyterephthalate

: 3958-60-9
2-nitrophenylmethyl bromide

: 1264669-97-7
dimethyl 2-((2-nitrobenzyl)oxy)terephthalate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 85 ℃; for 2h;
DOI:10.1002/anie.201004736

Reference yield:

: 636-94-2
2-hydroxyterephthalic acid

: 1264669-97-7
dimethyl 2-((2-nitrobenzyl)oxy)terephthalate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 80 °C

With sulfuric acid; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1039/c7cc02709e

Reference yield:

: 10312-55-7
3-aminoterephthalic acid

: 1264669-97-7
dimethyl 2-((2-nitrobenzyl)oxy)terephthalate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide; sodium nitrite; hydrogenchloride / water / 4 h / 10 °C

1.2: 12 h / 85 °C

2.1: sulfuric acid / Reflux

3.1: potassium carbonate / N,N-dimethyl-formamide / 80 °C

With hydrogenchloride; sulfuric acid; potassium carbonate; sodium hydroxide; sodium nitrite; In water; N,N-dimethyl-formamide;
DOI:10.1039/c7cc02709e