Technology Process of C21H24N10O6
There total 7 articles about C21H24N10O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride; acetic acid;
In
tetrahydrofuran;
at 20 ℃;
for 2.5h;
DOI:10.1021/cb200510k
- Guidance literature:
-
Multi-step reaction with 7 steps
1: N,N-dimethyl-formamide / 6 h / 20 °C
2: di-isopropyl azodicarboxylate; triphenylphosphine / 1,4-dioxane / 16 h / 20 °C
3: dmap / dichloromethane / 0.5 h / 0 °C
4: 18-crown-6 ether; potassium trifluoroacetate; N-ethyl-N,N-diisopropylamine / toluene / 16 h / 80 °C
5: dmap; triethylamine / dichloromethane / 0.25 h / 0 °C
6: lithium azide / N,N-dimethyl-formamide / 16 h / 20 °C
7: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2.5 h / 20 °C
With
dmap; lithium azide; 18-crown-6 ether; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; potassium trifluoroacetate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/cb200510k
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 18-crown-6 ether; potassium trifluoroacetate; N-ethyl-N,N-diisopropylamine / toluene / 16 h / 80 °C
2: dmap; triethylamine / dichloromethane / 0.25 h / 0 °C
3: lithium azide / N,N-dimethyl-formamide / 16 h / 20 °C
4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2.5 h / 20 °C
With
dmap; lithium azide; 18-crown-6 ether; tetrabutyl ammonium fluoride; potassium trifluoroacetate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/cb200510k