diphenyl (4-bromophenyl)-[5-(2-methoxyethylthio)-1,3,4-thiadiazol-2-ylamino]methylphosphonate

Base Information

Chemical Name:diphenyl (4-bromophenyl)-[5-(2-methoxyethylthio)-1,3,4-thiadiazol-2-ylamino]methylphosphonate
CAS No.:1519010-90-2
Molecular Formula:C₂₄H₂₃BrN₃O₄PS₂
Molecular Weight:592.474
Hs Code.:

Synonyms:diphenyl (4-bromophenyl)-[5-(2-methoxyethylthio)-1,3,4-thiadiazol-2-ylamino]methylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenyl (4-bromophenyl)-[5-(2-methoxyethylthio)-1,3,4-thiadiazol-2-ylamino]methylphosphonate

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Technology Process of diphenyl (4-bromophenyl)-[5-(2-methoxyethylthio)-1,3,4-thiadiazol-2-ylamino]methylphosphonate

There total 3 articles about diphenyl (4-bromophenyl)-[5-(2-methoxyethylthio)-1,3,4-thiadiazol-2-ylamino]methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 627-42-9
2-chloroethyl methyl ether

: 1519010-78-6
C₂₁H₁₇BrN₃O₃PS₂

: 1519010-90-2
diphenyl (4-bromophenyl)-[5-(2-methoxyethylthio)-1,3,4-thiadiazol-2-ylamino]methylphosphonate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 - 70 ℃;
DOI:10.1080/10426507.2013.797417

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1519010-90-2
diphenyl (4-bromophenyl)-[5-(2-methoxyethylthio)-1,3,4-thiadiazol-2-ylamino]methylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: perchloric acid / acetonitrile / 0.25 h / Reflux

1.2: 6 h / 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 20 - 70 °C

With perchloric acid; potassium carbonate; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1080/10426507.2013.797417

Reference yield:

: 101-02-0
triphenyl phosphite

: 1519010-90-2
diphenyl (4-bromophenyl)-[5-(2-methoxyethylthio)-1,3,4-thiadiazol-2-ylamino]methylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: perchloric acid / acetonitrile / 0.25 h / Reflux

1.2: 6 h / 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 20 - 70 °C

With perchloric acid; potassium carbonate; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1080/10426507.2013.797417