Technology Process of C84H104O6
There total 6 articles about C84H104O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N,N,N,N,-tetramethylethylenediamine; oxygen; copper(l) chloride;
In
para-xylene;
at 130 ℃;
for 7h;
DOI:10.1055/s-2002-32987
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 99 percent / NaH; TBAI / dimethylformamide / 19 h / 20 °C
2: 93 percent / CuCl; O2; TMEDA / acetone / 15 h / 60 °C
3: 88 percent / DDQ; aq. phosphate buffer / CH2Cl2 / 1.5 h / 0 °C / pH 7.2
4: 58 percent / NaH / dimethylsulfoxide / 6 h / 60 °C
5: 46 percent / CuCl; TMEDA; O2 / p-xylene / 7 h / 130 °C
With
phosphate buffer; N,N,N,N,-tetramethylethylenediamine; oxygen; tetra-(n-butyl)ammonium iodide; sodium hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; copper(l) chloride;
In
dichloromethane; para-xylene; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
2: Glaser acetylene coupling / 5: Glaser acetylene coupling;
DOI:10.1055/s-2002-32987
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 99 percent / NaH; TBAI / dimethylformamide / 19 h / 20 °C
2: 93 percent / CuCl; O2; TMEDA / acetone / 15 h / 60 °C
3: 88 percent / DDQ; aq. phosphate buffer / CH2Cl2 / 1.5 h / 0 °C / pH 7.2
4: 58 percent / NaH / dimethylsulfoxide / 6 h / 60 °C
5: 46 percent / CuCl; TMEDA; O2 / p-xylene / 7 h / 130 °C
With
phosphate buffer; N,N,N,N,-tetramethylethylenediamine; oxygen; tetra-(n-butyl)ammonium iodide; sodium hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; copper(l) chloride;
In
dichloromethane; para-xylene; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
2: Glaser acetylene coupling / 5: Glaser acetylene coupling;
DOI:10.1055/s-2002-32987
