(R)-methyl 3-(benzylthio)-2-(2-(4-((2-sulfamoylbenzo[d]thiazol-6-yloxy)methyl)-1H-1,2,3-triazol-1-yl)acetamido)propanoate

Base Information

Chemical Name:(R)-methyl 3-(benzylthio)-2-(2-(4-((2-sulfamoylbenzo[d]thiazol-6-yloxy)methyl)-1H-1,2,3-triazol-1-yl)acetamido)propanoate
CAS No.:1071472-23-5
Molecular Formula:C₂₃H₂₄N₆O₆S₃
Molecular Weight:576.678
Hs Code.:

Synonyms:(R)-methyl 3-(benzylthio)-2-(2-(4-((2-sulfamoylbenzo[d]thiazol-6-yloxy)methyl)-1H-1,2,3-triazol-1-yl)acetamido)propanoate

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Chemical Property of (R)-methyl 3-(benzylthio)-2-(2-(4-((2-sulfamoylbenzo[d]thiazol-6-yloxy)methyl)-1H-1,2,3-triazol-1-yl)acetamido)propanoate

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Technology Process of (R)-methyl 3-(benzylthio)-2-(2-(4-((2-sulfamoylbenzo[d]thiazol-6-yloxy)methyl)-1H-1,2,3-triazol-1-yl)acetamido)propanoate

There total 5 articles about (R)-methyl 3-(benzylthio)-2-(2-(4-((2-sulfamoylbenzo[d]thiazol-6-yloxy)methyl)-1H-1,2,3-triazol-1-yl)acetamido)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: (R)-2-(2-Azido-acetylamino)-3-benzylsulfanyl-propionic acid methyl ester

: 1071474-90-2
6-(prop-2-ynyloxy)benzo[d]thiazole-2-sulfonamide

: 1071472-23-5
(R)-methyl 3-(benzylthio)-2-(2-(4-((2-sulfamoylbenzo[d]thiazol-6-yloxy)methyl)-1H-1,2,3-triazol-1-yl)acetamido)propanoate

Guidance literature:: With copper(II) sulfate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 24h; pH=7.4; Aqueous phosphate buffer;

Reference yield:

: 452-35-7
6-ethoxybenzothiazole-2-sulfonamide

: 1071472-23-5
(R)-methyl 3-(benzylthio)-2-(2-(4-((2-sulfamoylbenzo[d]thiazol-6-yloxy)methyl)-1H-1,2,3-triazol-1-yl)acetamido)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: aluminum (III) chloride / dichloromethane / 24 h / 0 - 20 °C

2.1: sodium hydroxide / methanol; N,N-dimethyl-formamide / 0.75 h / 23 °C

2.2: 2.5 h

3.1: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol / 24 h / 20 °C / pH 7.4 / Aqueous phosphate buffer

With aluminum (III) chloride; sodium hydroxide; copper(II) sulfate; sodium L-ascorbate; In methanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 29927-14-8
6-hydroxy-2-benzothiazolesulfonamide

: 1071472-23-5
(R)-methyl 3-(benzylthio)-2-(2-(4-((2-sulfamoylbenzo[d]thiazol-6-yloxy)methyl)-1H-1,2,3-triazol-1-yl)acetamido)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / methanol; N,N-dimethyl-formamide / 0.75 h / 23 °C

1.2: 2.5 h

2.1: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol / 24 h / 20 °C / pH 7.4 / Aqueous phosphate buffer

With sodium hydroxide; copper(II) sulfate; sodium L-ascorbate; In methanol; water; N,N-dimethyl-formamide; tert-butyl alcohol;