methyl 4-(4-methyl-1-(4-(4-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)pent-1-en-2-yl)benzoate

Base Information

Chemical Name:methyl 4-(4-methyl-1-(4-(4-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)pent-1-en-2-yl)benzoate
CAS No.:1393126-61-8
Molecular Formula:C₂₄H₂₃F₃N₂O₂
Molecular Weight:428.454
Hs Code.:

Synonyms:methyl 4-(4-methyl-1-(4-(4-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)pent-1-en-2-yl)benzoate

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Chemical Property of methyl 4-(4-methyl-1-(4-(4-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)pent-1-en-2-yl)benzoate

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Technology Process of methyl 4-(4-methyl-1-(4-(4-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)pent-1-en-2-yl)benzoate

There total 4 articles about methyl 4-(4-methyl-1-(4-(4-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)pent-1-en-2-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.5%

: 1393126-60-7
methyl 4-(1-(4-bromophenyl)-4-methylpent-1-en-2-yl)benzoate

: 52222-73-8
4-(trifluoromethyl)-1H-pyrazole

: 1393126-61-8
methyl 4-(4-methyl-1-(4-(4-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)pent-1-en-2-yl)benzoate

Guidance literature:: With potassium carbonate; copper(l) iodide; 8-quinolinol; In dimethyl sulfoxide; at 90 ℃; for 18h; Inert atmosphere;

Reference yield:

: 1571-08-0
methyl 4-formylbenzoate

: 1393126-61-8
methyl 4-(4-methyl-1-(4-(4-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)pent-1-en-2-yl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 0 - 20 °C

2.1: pyridinium chlorochromate / dichloromethane / 48 h / 0 - 20 °C

3.1: lithium hexamethyldisilazane / toluene / 1 h / 0 - 20 °C

3.2: 18 h

4.1: potassium carbonate / copper(l) iodide; 8-quinolinol / dimethyl sulfoxide / 18 h / 90 °C / Inert atmosphere

With potassium carbonate; pyridinium chlorochromate; lithium hexamethyldisilazane; copper(l) iodide; 8-quinolinol; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene; 1.1: Grignard Reaction;

Reference yield:

: 100757-91-3
1-(p-methoxycarbonylphenyl)-3-methyl-1-butanol

: 1393126-61-8
methyl 4-(4-methyl-1-(4-(4-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)pent-1-en-2-yl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridinium chlorochromate / dichloromethane / 48 h / 0 - 20 °C

2.1: lithium hexamethyldisilazane / toluene / 1 h / 0 - 20 °C

2.2: 18 h

3.1: potassium carbonate / copper(l) iodide; 8-quinolinol / dimethyl sulfoxide / 18 h / 90 °C / Inert atmosphere

With potassium carbonate; pyridinium chlorochromate; lithium hexamethyldisilazane; copper(l) iodide; 8-quinolinol; In dichloromethane; dimethyl sulfoxide; toluene;