1-(4-(benzyloxy)phenethyl)-6-methoxy-3,7-bis(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole

Base Information

Chemical Name:1-(4-(benzyloxy)phenethyl)-6-methoxy-3,7-bis(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole
CAS No.:1269631-72-2
Molecular Formula:C₄₄H₄₆BNO₆
Molecular Weight:695.663
Hs Code.:

Synonyms:1-(4-(benzyloxy)phenethyl)-6-methoxy-3,7-bis(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole

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Chemical Property of 1-(4-(benzyloxy)phenethyl)-6-methoxy-3,7-bis(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole

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Technology Process of 1-(4-(benzyloxy)phenethyl)-6-methoxy-3,7-bis(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole

There total 13 articles about 1-(4-(benzyloxy)phenethyl)-6-methoxy-3,7-bis(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1269631-67-5
1-(4-(benzyloxy)phenethyl)-4-bromo-6-methoxy-3,7-bis(4-methoxyphenyl)-1H-indole

: 73183-34-3
bis(pinacol)diborane

: 1269631-72-2
1-(4-(benzyloxy)phenethyl)-6-methoxy-3,7-bis(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; for 3h; Reflux;
DOI:10.1002/asia.201000544

Reference yield:

: 1246523-50-1
4-bromo-6-methoxy-3,7-bis-(4-methoxy-phenyl)-2,3-dihydro-1H-indole

: 1269631-72-2
1-(4-(benzyloxy)phenethyl)-6-methoxy-3,7-bis(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 1 h / 20 °C

2.1: potassium hydroxide / N,N-dimethyl-formamide / 0.17 h / 20 °C

2.2: 2 h

3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,4-dioxane / 3 h / Reflux

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium hydroxide; In 1,4-dioxane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/asia.201000544

Reference yield:

: 1246523-51-2
4-bromo-6-methoxy-3,7-bis-(4-methoxy-phenyl)-1H-indole

: 1269631-72-2
1-(4-(benzyloxy)phenethyl)-6-methoxy-3,7-bis(4-methoxyphenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / N,N-dimethyl-formamide / 0.17 h / 20 °C

1.2: 2 h

2.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,4-dioxane / 3 h / Reflux

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; potassium hydroxide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1002/asia.201000544