(+)-{R-[R(R)]}-{4-[4-(4-oxiranyl)butoxy]phenoxy}butyloxirane

Base Information

Chemical Name:(+)-{R-[R*(R*)]}-{4-[4-(4-oxiranyl)butoxy]phenoxy}butyloxirane
CAS No.:173427-92-4
Molecular Formula:C₁₈H₂₆O₄
Molecular Weight:306.402
Hs Code.:

Synonyms:(+)-{R-[R*(R*)]}-{4-[4-(4-oxiranyl)butoxy]phenoxy}butyloxirane

Suppliers and Price of (+)-{R-[R*(R*)]}-{4-[4-(4-oxiranyl)butoxy]phenoxy}butyloxirane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-{R-[R*(R*)]}-{4-[4-(4-oxiranyl)butoxy]phenoxy}butyloxirane

Chemical Property:

Purity/Quality:

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Technology Process of (+)-{R-[R*(R*)]}-{4-[4-(4-oxiranyl)butoxy]phenoxy}butyloxirane

There total 5 articles about (+)-{R-[R*(R*)]}-{4-[4-(4-oxiranyl)butoxy]phenoxy}butyloxirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1445-45-0
Trimethyl orthoacetate

: 506-96-7
Acetyl bromide

: 173427-91-3
-6,6'-<1,4-phenylenebis(oxy)>bis-1,2-hexanediol

: 173427-92-4
(+)-{R-[R*(R*)]}-{4-[4-(4-oxiranyl)butoxy]phenoxy}butyloxirane

Guidance literature:: With pyridinium p-toluenesulfonate; potassium carbonate; In methanol; dichloromethane;

Reference yield:

: 173427-91-3
-6,6'-<1,4-phenylenebis(oxy)>bis-1,2-hexanediol

: 173427-92-4
(+)-{R-[R*(R*)]}-{4-[4-(4-oxiranyl)butoxy]phenoxy}butyloxirane

Guidance literature:: With Acetyl bromide; pyridinium p-toluenesulfonate; potassium carbonate; trimethyl orthoformate; Yield given. Multistep reaction;
DOI:10.1021/ja953781q

Reference yield:

: 18922-04-8
6-iodohex-1-ene

: 173427-92-4
(+)-{R-[R*(R*)]}-{4-[4-(4-oxiranyl)butoxy]phenoxy}butyloxirane

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent

2: 62 percent / AD-mix-β

3: 1.) CH(OME)3, PPTS, 2.) AcBr, 3.) K₂CO₃

With Acetyl bromide; AD-mix-β; pyridinium p-toluenesulfonate; potassium carbonate; trimethyl orthoformate;
DOI:10.1021/ja953781q