methanesulfonic acid 2-benzyloxymethyl-3-methanesulfonyloxypropyl ester

Base Information

Chemical Name:methanesulfonic acid 2-benzyloxymethyl-3-methanesulfonyloxypropyl ester
CAS No.:1122410-38-1
Molecular Formula:C₁₃H₂₀O₇S₂
Molecular Weight:352.43
Hs Code.:

Synonyms:methanesulfonic acid 2-benzyloxymethyl-3-methanesulfonyloxypropyl ester

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Chemical Property of methanesulfonic acid 2-benzyloxymethyl-3-methanesulfonyloxypropyl ester

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Technology Process of methanesulfonic acid 2-benzyloxymethyl-3-methanesulfonyloxypropyl ester

There total 4 articles about methanesulfonic acid 2-benzyloxymethyl-3-methanesulfonyloxypropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 75-75-2,98527-29-8
methanesulfonic acid

: 117087-18-0
2-((benzyloxy)methyl)propane-1,3-diol

: 1122410-38-1
methanesulfonic acid 2-benzyloxymethyl-3-methanesulfonyloxypropyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 1.5h;
DOI:10.1016/j.ejmech.2008.02.021

Reference yield: 84.0%

: 117087-18-0
2-((benzyloxy)methyl)propane-1,3-diol

: 124-63-0
methanesulfonyl chloride

: 1122410-38-1
methanesulfonic acid 2-benzyloxymethyl-3-methanesulfonyloxypropyl ester

Guidance literature:: 2-[(benzyloxy)methyl]propane-1,3-diol; With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;

methanesulfonyl chloride; In dichloromethane; at 0 ℃; for 3h;

Reference yield:

: 117087-17-9
5-[(benzyloxy)methyl]-2,2-dimethyl-1,3-dioxane

: 1122410-38-1
methanesulfonic acid 2-benzyloxymethyl-3-methanesulfonyloxypropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / methanol / 1 h / 20 °C

2.1: triethylamine / dichloromethane / 0.5 h / 0 °C

2.2: 3 h / 0 °C

With toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane;