[2-(N-(2-pyridyl)carbamoyl)-pyridine]bis-triphenylphosphine(2,2'-bipyridine)ruthenium(II) perchlorate

Base Information

• Chemical Name: [2-(N-(2-pyridyl)carbamoyl)-pyridine]bis-triphenylphosphine(2,2'-bipyridine)ruthenium(II) perchlorate
• CAS No.: 364041-99-6
• Molecular Formula: C₅₇H₄₆N₅OP₂Ru*ClO₄
• Molecular Weight: 1079.49
• Mol file: 364041-99-6.mol

Synonyms:[2-(N-(2-pyridyl)carbamoyl)-pyridine]bis-triphenylphosphine(2,2'-bipyridine)ruthenium(II) perchlorate

Chemical Property of [2-(N-(2-pyridyl)carbamoyl)-pyridine]bis-triphenylphosphine(2,2'-bipyridine)ruthenium(II) perchlorate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of [2-(N-(2-pyridyl)carbamoyl)-pyridine]bis-triphenylphosphine(2,2'-bipyridine)ruthenium(II) perchlorate

There total 1 articles about [2-(N-(2-pyridyl)carbamoyl)-pyridine]bis-triphenylphosphine(2,2'-bipyridine)ruthenium(II) perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

[2,2]bipyridinyl (366-18-7) + dichlorobis-triphenylphosphine[2-(N-(2-pyridinium-2-yl)-carbamoyl-N(-))-pyridine]ruthenium(II) (364041-97-4) + sodium perchlorate → [2-(N-(2-pyridyl)carbamoyl)-pyridine]bis-triphenylphosphine(2,2'-bipyridine)ruthenium(II) perchlorate (364041-99-6)

Guidance literature:

With triethylammonium; In ethanol; equimol., refluxed for 2 h, filtered, concd., cooled, aq. NaClO4 added; ppt. filtered, wached thoroughly (water), dried (CaCl2); elem. anal.;

DOI:10.1016/S0277-5387(01)00706-9

upstream raw materials:

[2,2]bipyridinyl

dichlorobis-triphenylphosphine[2-(N-(2-pyridinium-2-yl)-carbamoyl-N(-))-pyridine]ruthenium(II)