(E)-ethyl 3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)but-2-enoate

Base Information

Chemical Name:(E)-ethyl 3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)but-2-enoate
CAS No.:1613169-23-5
Molecular Formula:C₁₈H₂₅BO₄
Molecular Weight:316.205
Hs Code.:

Synonyms:(E)-ethyl 3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)but-2-enoate

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Chemical Property of (E)-ethyl 3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)but-2-enoate

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Technology Process of (E)-ethyl 3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)but-2-enoate

There total 1 articles about (E)-ethyl 3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)but-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 352287-96-8
(E)-3-(4-bromophenyl)but-2-enoic acid ethyl ester

: 73183-34-3
bis(pinacol)diborane

: 1613169-23-5
(E)-ethyl 3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)but-2-enoate

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; at 110 ℃; for 5h; Inert atmosphere;

Reference yield:

: 1613169-23-5
(E)-ethyl 3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)but-2-enoate

: 1613169-24-6
ethyl 3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)butanoate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; for 6h; under 3102.97 Torr;

Reference yield:

: 1613169-23-5
(E)-ethyl 3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)but-2-enoate

: 1613169-22-4
3-[4-(tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]butanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 6 h / 3102.97 Torr

2: lithium hydroxide monohydrate; hydrogen / tetrahydrofuran / 15 h / 20 °C

With lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol;