N-[chloro-(2,2-dichloro-1-methyl-cyclopropyl)methylene]-N'-(2,6-dichloro-4-trifluoromethyl-phenyl)-hydrazine

Base Information

Chemical Name:N-[chloro-(2,2-dichloro-1-methyl-cyclopropyl)methylene]-N'-(2,6-dichloro-4-trifluoromethyl-phenyl)-hydrazine
CAS No.:156819-69-1
Molecular Formula:C₁₂H₈Cl₅F₃N₂
Molecular Weight:414.469
Hs Code.:

Synonyms:N-[chloro-(2,2-dichloro-1-methyl-cyclopropyl)methylene]-N'-(2,6-dichloro-4-trifluoromethyl-phenyl)-hydrazine

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Chemical Property of N-[chloro-(2,2-dichloro-1-methyl-cyclopropyl)methylene]-N'-(2,6-dichloro-4-trifluoromethyl-phenyl)-hydrazine

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Technology Process of N-[chloro-(2,2-dichloro-1-methyl-cyclopropyl)methylene]-N'-(2,6-dichloro-4-trifluoromethyl-phenyl)-hydrazine

There total 2 articles about N-[chloro-(2,2-dichloro-1-methyl-cyclopropyl)methylene]-N'-(2,6-dichloro-4-trifluoromethyl-phenyl)-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 156819-60-2
2,2-dichloro-1-methylcyclopropyl carboxylic acid N'-[2,6-dichloro-4-(trifluoromethyl)phenyl]hydrazide

: 156819-69-1
N-[chloro-(2,2-dichloro-1-methyl-cyclopropyl)methylene]-N'-(2,6-dichloro-4-trifluoromethyl-phenyl)-hydrazine

Guidance literature:: With thionyl chloride; In toluene; for 3h; Heating / reflux;

Reference yield:

: 56447-09-7
2,2-dichloro-1-methyl-cyclopropanoyl chloride

: 86398-94-9
2,6-dichloro-4-(trifluoromethyl)phenyl hydrazine

: 156819-69-1
N-[chloro-(2,2-dichloro-1-methyl-cyclopropyl)methylene]-N'-(2,6-dichloro-4-trifluoromethyl-phenyl)-hydrazine

Guidance literature:: 2,2-dichloro-1-methyl-cyclopropanoyl chloride; 2,6-dichloro-4-(trifluoromethyl)phenyl hydrazine; In toluene; at 15 - 25 ℃; for 0.5h;

With sodium hydroxide; In water; toluene; at 80 ℃;

With thionyl chloride; In toluene; at 110 ℃; for 3h; Heating / reflux;

Reference yield: 60.0%

: 156819-69-1
N-[chloro-(2,2-dichloro-1-methyl-cyclopropyl)methylene]-N'-(2,6-dichloro-4-trifluoromethyl-phenyl)-hydrazine

: 109-77-3
malononitrile

: 5-AMINO-3-(2,2-DICHLORO-1-METHYLCYCLOPROPYL)-1-[2,6-DICHLORO-4-(TRIFLUOROMETHYL)PHENYL]-1H-PYRAZOLE-4-CARBONITRILE

Guidance literature:: malononitrile; With sodium hydride; In tetrahydrofuran;

N-[chloro-(2,2-dichloro-1-methyl-cyclopropyl)methylene]-N'-(2,6-dichloro-4-trifluoromethyl-phenyl)-hydrazine; In tetrahydrofuran; at 0 - 20 ℃; for 2h;