C₁₄H₁₁Cl₂NO

Base Information

Chemical Name:C₁₄H₁₁Cl₂NO
CAS No.:1372788-46-9
Molecular Formula:C₁₄H₁₁Cl₂NO
Molecular Weight:280.153
Hs Code.:

C<sub>14</sub>H<sub>11</sub>Cl<sub>2</sub>NO

Synonyms:C₁₄H₁₁Cl₂NO

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Chemical Property of C₁₄H₁₁Cl₂NO

Chemical Property:

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Technology Process of C₁₄H₁₁Cl₂NO

There total 3 articles about C₁₄H₁₁Cl₂NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 319-39-1
N-(p-chlorophenyl)-o-chlorobenzamide

: 74-88-4
methyl iodide

: 1372788-46-9
C₁₄H₁₁Cl₂NO

Guidance literature:: N-(p-chlorophenyl)-o-chlorobenzamide; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; Inert atmosphere;

methyl iodide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.201101400

Reference yield:

: 609-65-4
o-chlorobenzoyl chloride

: 1372788-46-9
C₁₄H₁₁Cl₂NO

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / ethyl acetate / 1 h / 0 - 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0 °C / Inert atmosphere

2.2: 2 h / 0 - 20 °C / Inert atmosphere

With sodium hydride; triethylamine; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201101400

Reference yield:

: 118-91-2
ortho-chlorobenzoic acid

: 1372788-46-9
C₁₄H₁₁Cl₂NO

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / 5 h / Reflux

2.1: triethylamine / ethyl acetate / 1 h / 0 - 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0 °C / Inert atmosphere

3.2: 2 h / 0 - 20 °C / Inert atmosphere

With thionyl chloride; sodium hydride; triethylamine; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201101400