3-benzenesulfonyl-4-(3-(4-(tert-butyl(dimethyl)silyloxy)phenyl)propoxy)furoxan

Base Information

Chemical Name:3-benzenesulfonyl-4-(3-(4-(tert-butyl(dimethyl)silyloxy)phenyl)propoxy)furoxan
CAS No.:893403-87-7
Molecular Formula:C₂₃H₃₀N₂O₆SSi
Molecular Weight:490.653
Hs Code.:

Synonyms:3-benzenesulfonyl-4-(3-(4-(tert-butyl(dimethyl)silyloxy)phenyl)propoxy)furoxan

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Chemical Property of 3-benzenesulfonyl-4-(3-(4-(tert-butyl(dimethyl)silyloxy)phenyl)propoxy)furoxan

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Technology Process of 3-benzenesulfonyl-4-(3-(4-(tert-butyl(dimethyl)silyloxy)phenyl)propoxy)furoxan

There total 10 articles about 3-benzenesulfonyl-4-(3-(4-(tert-butyl(dimethyl)silyloxy)phenyl)propoxy)furoxan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 66074-00-8
3,4-bis(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide

: 215776-67-3
3-[4-(tert-butyl-dimethyl-silanyloxy)phenyl]propan-1-ol

: 893403-87-7
3-benzenesulfonyl-4-(3-(4-(tert-butyl(dimethyl)silyloxy)phenyl)propoxy)furoxan

Guidance literature:: 3-[4-(tert-butyl-dimethyl-silanyloxy)phenyl]propan-1-ol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

3,4-bis(phenylsulfonyl)-1,2,5-oxadiazole 2-oxide; In tetrahydrofuran; at 30 ℃;
DOI:10.1021/jm0510530

Reference yield:

: 5597-50-2
3-(4-hydroxyphenyl)propionic acid methyl ester

: 893403-87-7
3-benzenesulfonyl-4-(3-(4-(tert-butyl(dimethyl)silyloxy)phenyl)propoxy)furoxan

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.33 h / 0 - 20 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran;

Reference yield:

: 120743-99-9
p-[(tert-butyldimethylsilyl)oxy]benzaldehyde

: 893403-87-7
3-benzenesulfonyl-4-(3-(4-(tert-butyl(dimethyl)silyloxy)phenyl)propoxy)furoxan

Guidance literature:: Multi-step reaction with 4 steps

1.1: t-BuOK / tetrahydrofuran / -78 °C

1.2: tetrahydrofuran / -78 - 20 °C

2.1: 96 percent / H₂ / Pd/C / ethanol / 3 h / atmospheric pressure

3.1: 100 percent / LiAlH₄ / tetrahydrofuran / 1.5 h / 20 °C

4.1: NaH / tetrahydrofuran / 0.5 h / 0 °C

4.2: 54 percent / tetrahydrofuran / 30 °C

With lithium aluminium tetrahydride; potassium tert-butylate; hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1021/jm0510530