Butyl-[(2E,4E,6E,8E)-3-tert-butyl-7-methyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine

Base Information

• Chemical Name: Butyl-[(2E,4E,6E,8E)-3-tert-butyl-7-methyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine
• CAS No.: 115018-97-8
• Molecular Formula: C₂₇H₄₃N
• Molecular Weight: 381.645

Synonyms:Butyl-[(2E,4E,6E,8E)-3-tert-butyl-7-methyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine

Chemical Property of Butyl-[(2E,4E,6E,8E)-3-tert-butyl-7-methyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine

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Technology Process of Butyl-[(2E,4E,6E,8E)-3-tert-butyl-7-methyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine

There total 1 articles about Butyl-[(2E,4E,6E,8E)-3-tert-butyl-7-methyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

13-tert-butyl-13-cis-retinal (106190-63-0) + N-butylamine (109-73-9,85404-21-3) → 1-Butyl-4-tert-butyl-2-[(1E,3E)-2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-buta-1,3-dienyl]-1,2-dihydro-pyridine (115018-98-9) + Butyl-[(2E,4E,6E,8E)-3-tert-butyl-7-methyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine (115018-97-8)

Guidance literature:

With 4 A molecular sieve; In ethanol; at 0 ℃; for 0.166667h; Title compound not separated from byproducts;

DOI:10.1021/ja00193a043

Reference yield:

Butyl-[(2E,4E,6E,8E)-3-tert-butyl-7-methyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine (115018-97-8) → 1-Butyl-4-tert-butyl-2-[(1E,3E)-2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-buta-1,3-dienyl]-1,2-dihydro-pyridine (115018-98-9)

Guidance literature:

In benzene-d6; at 23 ℃; the half-life for the electrocyclization reaction;

DOI:10.1021/ja00193a043

upstream raw materials:

13-tert-butyl-13-cis-retinal

N-butylamine

Downstream raw materials:

1-Butyl-4-tert-butyl-2-[(1E,3E)-2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-buta-1,3-dienyl]-1,2-dihydro-pyridine

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