(S)-3-(methoxymethoxy)-3-((4R,5R)-5-((R)-4-tert-butyldiphenylsilyloxypentyl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-1-ol

Base Information

Chemical Name:(S)-3-(methoxymethoxy)-3-((4R,5R)-5-((R)-4-tert-butyldiphenylsilyloxypentyl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-1-ol
CAS No.:1427278-68-9
Molecular Formula:C₃₁H₄₈O₆Si
Molecular Weight:544.804
Hs Code.:

Synonyms:(S)-3-(methoxymethoxy)-3-((4R,5R)-5-((R)-4-tert-butyldiphenylsilyloxypentyl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-1-ol

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Chemical Property of (S)-3-(methoxymethoxy)-3-((4R,5R)-5-((R)-4-tert-butyldiphenylsilyloxypentyl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-1-ol

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Technology Process of (S)-3-(methoxymethoxy)-3-((4R,5R)-5-((R)-4-tert-butyldiphenylsilyloxypentyl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-1-ol

There total 2 articles about (S)-3-(methoxymethoxy)-3-((4R,5R)-5-((R)-4-tert-butyldiphenylsilyloxypentyl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1431985-93-1
C₃₁H₄₆O₆Si

: 1427278-68-9
(S)-3-(methoxymethoxy)-3-((4R,5R)-5-((R)-4-tert-butyldiphenylsilyloxypentyl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-1-ol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2013.02.033

Reference yield:

: 1388144-87-3
((R)-5-((4R,5R)-5-((S)-1-(methoxymethoxy)but-3-enyl)-2,2-dimethyl-1,3-dioxolan-4-yl)pentan-2-yloxy)(tert-butyl)diphenylsilane

: 1427278-68-9
(S)-3-(methoxymethoxy)-3-((4R,5R)-5-((R)-4-tert-butyldiphenylsilyloxypentyl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: osmium(VIII) oxide; sodium periodate; 4-methylmorpholine N-oxide / tetrahydrofuran; water; toluene / 3 h / 20 °C

2: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

With sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; water; toluene;
DOI:10.1016/j.tet.2013.02.033

Reference yield:

: 1427278-68-9
(S)-3-(methoxymethoxy)-3-((4R,5R)-5-((R)-4-tert-butyldiphenylsilyloxypentyl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-1-ol

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: C₃₈H₅₂N₄O₅SSi

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at -20 - 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tet.2013.02.033