C₂₁H₃₄O₃Si

Base Information

Chemical Name:C₂₁H₃₄O₃Si
CAS No.:1004540-05-9
Molecular Formula:C₂₁H₃₄O₃Si
Molecular Weight:362.585
Hs Code.:

C<sub>21</sub>H<sub>34</sub>O<sub>3</sub>Si

Synonyms:C₂₁H₃₄O₃Si

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Chemical Property of C₂₁H₃₄O₃Si

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Technology Process of C₂₁H₃₄O₃Si

There total 4 articles about C₂₁H₃₄O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 78592-77-5
(E)-4-tert-butyldimethylsilyloxy-1-iodo-2-methyl-1-butene

: 406940-46-3
(-)-(S)-2-(benzyloxy)-N-methoxy-N-methylpropanamide

: 1004540-05-9
C₂₁H₃₄O₃Si

Guidance literature:: (E)-4-tert-butyldimethylsilyloxy-1-iodo-2-methyl-1-butene; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 0.5h;

(-)-(S)-2-(benzyloxy)-N-methoxy-N-methylpropanamide; In diethyl ether; hexane; at -78 ℃; for 0.5h; Further stages.;
DOI:10.1021/ol702921x

Reference yield:

: 100-39-0
benzyl bromide

: 1004540-05-9
C₂₁H₃₄O₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: silver(l) oxide / dichloromethane / 48 h / 20 °C / Inert atmosphere

2.1: potassium hydroxide; water / ethanol / 0.5 h / 0 °C / Inert atmosphere

3.1: pivaloyl chloride; triethylamine / 0.5 h / 0 °C / Inert atmosphere

3.2: 16 h / 20 °C / Inert atmosphere

4.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -78 °C / Inert atmosphere

4.2: 0.01 h / -78 °C / Inert atmosphere

With n-butyllithium; water; pivaloyl chloride; triethylamine; potassium hydroxide; silver(l) oxide; In diethyl ether; ethanol; hexane; dichloromethane;
DOI:10.1021/acs.joc.7b00428

Reference yield:

: 33106-32-0
(S)-2-(benzyloxy)propanoic acid

: 1004540-05-9
C₂₁H₃₄O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: pivaloyl chloride; triethylamine / 0.5 h / 0 °C / Inert atmosphere

1.2: 16 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -78 °C / Inert atmosphere

2.2: 0.01 h / -78 °C / Inert atmosphere

With n-butyllithium; pivaloyl chloride; triethylamine; In diethyl ether; hexane;
DOI:10.1021/acs.joc.7b00428