benzyl (2,3,4,6-O-tetra-O-acetyl-β-D-galactopyranosyl)-(1-> 3)-2-acetamido-2-deoxy-6-O-trimethylacetyl-α-D-galactopyranoside

Base Information

Chemical Name:benzyl (2,3,4,6-O-tetra-O-acetyl-β-D-galactopyranosyl)-(1-> 3)-2-acetamido-2-deoxy-6-O-trimethylacetyl-α-D-galactopyranoside
CAS No.:161299-10-1
Molecular Formula:C₃₄H₄₇NO₁₆
Molecular Weight:725.744
Hs Code.:

Synonyms:benzyl (2,3,4,6-O-tetra-O-acetyl-β-D-galactopyranosyl)-(1-> 3)-2-acetamido-2-deoxy-6-O-trimethylacetyl-α-D-galactopyranoside

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Chemical Property of benzyl (2,3,4,6-O-tetra-O-acetyl-β-D-galactopyranosyl)-(1-> 3)-2-acetamido-2-deoxy-6-O-trimethylacetyl-α-D-galactopyranoside

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Technology Process of benzyl (2,3,4,6-O-tetra-O-acetyl-β-D-galactopyranosyl)-(1-> 3)-2-acetamido-2-deoxy-6-O-trimethylacetyl-α-D-galactopyranoside

There total 4 articles about benzyl (2,3,4,6-O-tetra-O-acetyl-β-D-galactopyranosyl)-(1-> 3)-2-acetamido-2-deoxy-6-O-trimethylacetyl-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 3282-30-2
pivaloyl chloride

: 90754-57-7,60831-31-4
benzyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1<*>3)-2-acetamido-2-deoxy-α-D-galactopyranoside

: 161299-10-1
benzyl (2,3,4,6-O-tetra-O-acetyl-β-D-galactopyranosyl)-(1-> 3)-2-acetamido-2-deoxy-6-O-trimethylacetyl-α-D-galactopyranoside

Guidance literature:: With pyridine; at 0 - 25 ℃; for 12h;
DOI:10.1016/S0008-6215(00)00080-X

Reference yield:

: 117182-56-6
benzyl 2-acetamide-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

: 161299-10-1
benzyl (2,3,4,6-O-tetra-O-acetyl-β-D-galactopyranosyl)-(1-> 3)-2-acetamido-2-deoxy-6-O-trimethylacetyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: Hg(CN)2 / benzene; nitromethane / 24 h / 40 - 45 °C

2: AcOH / H₂O / 1.5 h / 60 - 65 °C

3: 95 percent / pyridine / 12 h / 0 - 25 °C

With pyridine; mercury(II) cyanide; acetic acid; In nitromethane; water; benzene; 1: Substitution / 2: ether cleavage / 3: Acylation;
DOI:10.1016/S0008-6215(00)00080-X

Reference yield:

: 117181-30-3
benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranoside

: 161299-10-1
benzyl (2,3,4,6-O-tetra-O-acetyl-β-D-galactopyranosyl)-(1-> 3)-2-acetamido-2-deoxy-6-O-trimethylacetyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH / H₂O / 1.5 h / 60 - 65 °C

2: 95 percent / pyridine / 12 h / 0 - 25 °C

With pyridine; acetic acid; In water; 1: ether cleavage / 2: Acylation;
DOI:10.1016/S0008-6215(00)00080-X