methyl {6-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]-2,3-dihydro-benzofuran-3-yl}acetate

Base Information

Chemical Name:methyl {6-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]-2,3-dihydro-benzofuran-3-yl}acetate
CAS No.:1356600-64-0
Molecular Formula:C₂₇H₂₇NO₆
Molecular Weight:461.514
Hs Code.:

Synonyms:methyl {6-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]-2,3-dihydro-benzofuran-3-yl}acetate

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Chemical Property of methyl {6-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]-2,3-dihydro-benzofuran-3-yl}acetate

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Technology Process of methyl {6-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]-2,3-dihydro-benzofuran-3-yl}acetate

There total 7 articles about methyl {6-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]-2,3-dihydro-benzofuran-3-yl}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.1%

: 1356599-86-4
(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}phenyl)methanol

: 805250-17-3,1234474-58-8
(6-hydroxy-2,3-dihydro-benzofuran-3-yl)-acetic acid methyl ester

: 1356600-64-0
methyl {6-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]-2,3-dihydro-benzofuran-3-yl}acetate

Guidance literature:: With tributylphosphine; 1,1'-azodicarbonyl-dipiperidine; In toluene; at 0 - 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 25392-41-0
4-chloromethyl-7-hydroxycoumarin

: 1356600-64-0
methyl {6-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]-2,3-dihydro-benzofuran-3-yl}acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide; water / 2 h / Reflux

1.2: 20 °C

2.1: sulfuric acid / 4 h / Reflux

3.1: hydrogen / palladium 10% on activated carbon / methanol / 24 h / 20 °C / 1034.32 Torr

4.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 2 h / 0 - 20 °C / Inert atmosphere

With tributylphosphine; sulfuric acid; water; hydrogen; sodium hydroxide; 1,1'-azodicarbonyl-dipiperidine; palladium 10% on activated carbon; In methanol; toluene;

Reference yield:

: 108-46-3
recorcinol

: 1356600-64-0
methyl {6-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]-2,3-dihydro-benzofuran-3-yl}acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / 2 h / 0 - 20 °C

2.1: sodium hydroxide; water / 2 h / Reflux

2.2: 20 °C

3.1: sulfuric acid / 4 h / Reflux

4.1: hydrogen / palladium 10% on activated carbon / methanol / 24 h / 20 °C / 1034.32 Torr

5.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 2 h / 0 - 20 °C / Inert atmosphere

With tributylphosphine; sulfuric acid; water; hydrogen; sodium hydroxide; 1,1'-azodicarbonyl-dipiperidine; palladium 10% on activated carbon; In methanol; toluene;