2-(4-chlorobenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazol-5-yl thiocyanate

Base Information

Chemical Name:2-(4-chlorobenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazol-5-yl thiocyanate
CAS No.:1620897-91-7
Molecular Formula:C₁₉H₁₃ClN₄OS₂
Molecular Weight:412.923
Hs Code.:

Synonyms:2-(4-chlorobenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazol-5-yl thiocyanate

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Chemical Property of 2-(4-chlorobenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazol-5-yl thiocyanate

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Technology Process of 2-(4-chlorobenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazol-5-yl thiocyanate

There total 3 articles about 2-(4-chlorobenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazol-5-yl thiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1315275-38-7
2-(4-chlorobenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazole

: 333-20-0
potassium thioacyanate

: 1620897-91-7
2-(4-chlorobenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazol-5-yl thiocyanate

Guidance literature:: With bromine; In acetic acid; at 0 - 20 ℃; for 1.5h;
DOI:10.1016/j.ejmech.2014.07.054

Reference yield:

: 39181-43-6
5-[(4-chlorophenyl)methyl]-1,3,4-thiadiazol-2-amine

: 1620897-91-7
2-(4-chlorobenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazol-5-yl thiocyanate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / 10 - 12 h / Reflux

2: bromine / acetic acid / 1.5 h / 0 - 20 °C

With bromine; sodium carbonate; In acetic acid;
DOI:10.1016/j.ejmech.2014.07.054

Reference yield:

: 2632-13-5
2-Bromo-4'-methoxyacetophenone

: 1620897-91-7
2-(4-chlorobenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazol-5-yl thiocyanate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / 10 - 12 h / Reflux

2: bromine / acetic acid / 1.5 h / 0 - 20 °C

With bromine; sodium carbonate; In acetic acid;
DOI:10.1016/j.ejmech.2014.07.054