(R)-N-[(S)-(2,4-dichlorophenyl)(p-tolyl)methyl]-2-methylpropane-2-sulfinamide

Base Information

Chemical Name:(R)-N-[(S)-(2,4-dichlorophenyl)(p-tolyl)methyl]-2-methylpropane-2-sulfinamide
CAS No.:1345627-85-1
Molecular Formula:C₁₈H₂₁Cl₂NOS
Molecular Weight:370.343
Hs Code.:

Synonyms:(R)-N-[(S)-(2,4-dichlorophenyl)(p-tolyl)methyl]-2-methylpropane-2-sulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-N-[(S)-(2,4-dichlorophenyl)(p-tolyl)methyl]-2-methylpropane-2-sulfinamide

Chemical Property:

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Technology Process of (R)-N-[(S)-(2,4-dichlorophenyl)(p-tolyl)methyl]-2-methylpropane-2-sulfinamide

There total 2 articles about (R)-N-[(S)-(2,4-dichlorophenyl)(p-tolyl)methyl]-2-methylpropane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1015198-52-3
(R)-N-(2,4-dichlorophenyl)methylene-2-methylpropane-2-sulfinamide

: 4294-57-9
para-methylphenylmagnesium bromide

: (R)-N-[(R)-(2,4-dichlorophenyl)(p-tolyl)methyl]-2-methylpropane-2-sulfinamide

: 1345627-85-1
(R)-N-[(S)-(2,4-dichlorophenyl)(p-tolyl)methyl]-2-methylpropane-2-sulfinamide

Guidance literature:: (R)-N-(2,4-dichlorophenyl)methylene-2-methylpropane-2-sulfinamide; para-methylphenylmagnesium bromide; In tetrahydrofuran; toluene; at -20 - 20 ℃; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; water; toluene; optical yield given as %de; Saturated solution;
DOI:10.1016/j.ejmech.2011.08.030

Reference yield:

: 874-42-0
2,4-dichlorobenzaldeyhde

: 1345627-85-1
(R)-N-[(S)-(2,4-dichlorophenyl)(p-tolyl)methyl]-2-methylpropane-2-sulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium(IV) isopropylate / tetrahydrofuran / 6 h / 40 °C / Inert atmosphere

2.1: tetrahydrofuran; toluene / -20 - 20 °C / Inert atmosphere

2.2: Saturated solution

With titanium(IV) isopropylate; In tetrahydrofuran; toluene;
DOI:10.1016/j.ejmech.2011.08.030

Reference yield:

: 1345627-85-1
(R)-N-[(S)-(2,4-dichlorophenyl)(p-tolyl)methyl]-2-methylpropane-2-sulfinamide

: 1345627-89-5
(S)-(2,4-dichlorophenyl)(p-tolyl)methanamine

Guidance literature:: (R)-N-[(S)-(2,4-dichlorophenyl)(p-tolyl)methyl]-2-methylpropane-2-sulfinamide; With hydrogenchloride; In methanol; at 20 ℃; for 2h;

With sodium hydroxide; In diethyl ether; water;
DOI:10.1016/j.ejmech.2011.08.030