2--4-carbetoxyimidazole

Base Information

Chemical Name:2--4-carbetoxyimidazole
CAS No.:102151-68-8
Molecular Formula:C₁₉H₁₈N₂O₃
Molecular Weight:322.364
Hs Code.:

2-<p-(benzyloxy)phenyl>-4-carbetoxyimidazole

Synonyms:2--4-carbetoxyimidazole

Suppliers and Price of 2--4-carbetoxyimidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--4-carbetoxyimidazole

Chemical Property:

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Technology Process of 2--4-carbetoxyimidazole

There total 1 articles about 2--4-carbetoxyimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-03-6
ethyl iodide

: 102151-53-1
2-imidazole-4-carboxylic acid

: 102151-68-8
2--4-carbetoxyimidazole

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 60 deg C, 0.5 h, 2.) DMF, RT, ovrnight;
DOI:10.1021/jm00156a028

Reference yield: 90.0%

: 102151-68-8
2--4-carbetoxyimidazole

: 102151-69-9
4-carbethoxy-2-(4-hydroxyphenyl)imidazole

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; for 3h; under 1758.3 Torr;
DOI:10.1021/jm00156a028

Reference yield:

: 102151-68-8
2--4-carbetoxyimidazole

: 2-(4-{(S)-3-[2-(3,4-Dimethoxy-phenyl)-ethyl]-2-phenyl-oxazolidin-5-ylmethoxy}-phenyl)-3H-imidazole-4-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / H₂ / 10percent Pd/C / acetic acid / 3 h / 1758.3 Torr

2: 1.) NaH / 1.) DMF, 70 deg C, 15 min, 2.) DMF, 120 deg C, 18 h

With hydrogen; sodium hydride; palladium on activated charcoal; In acetic acid;
DOI:10.1021/jm00156a028