carbonic acid 2-bromo-3-tert-butoxycarbonyloxy-6-formyl-phenyl ester tert-butyl ester

Base Information

Chemical Name:carbonic acid 2-bromo-3-tert-butoxycarbonyloxy-6-formyl-phenyl ester tert-butyl ester
CAS No.:680997-58-4
Molecular Formula:C₁₇H₂₁BrO₇
Molecular Weight:417.254
Hs Code.:

Synonyms:carbonic acid 2-bromo-3-tert-butoxycarbonyloxy-6-formyl-phenyl ester tert-butyl ester

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Chemical Property of carbonic acid 2-bromo-3-tert-butoxycarbonyloxy-6-formyl-phenyl ester tert-butyl ester

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Technology Process of carbonic acid 2-bromo-3-tert-butoxycarbonyloxy-6-formyl-phenyl ester tert-butyl ester

There total 1 articles about carbonic acid 2-bromo-3-tert-butoxycarbonyloxy-6-formyl-phenyl ester tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 131088-01-2
3-bromo-2,4-dihydroxybenzaldehyde

: 680997-58-4
carbonic acid 2-bromo-3-tert-butoxycarbonyloxy-6-formyl-phenyl ester tert-butyl ester

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 8h;
DOI:10.1021/ol0498592

Reference yield: 90.0%

: 10442-39-4
tetra-n-butylammonium cyanide

: 680997-58-4
carbonic acid 2-bromo-3-tert-butoxycarbonyloxy-6-formyl-phenyl ester tert-butyl ester

: 680997-63-1
carbonic acid 2-bromo-4-cyanomethyl-3-hydroxy-phenyl ester tert-butyl ester

Guidance literature:: carbonic acid 2-bromo-3-tert-butoxycarbonyloxy-6-formyl-phenyl ester tert-butyl ester; With sodium tetrahydroborate; In tetrahydrofuran; water; at 0 ℃; for 0.00333333h;

tetra-n-butylammonium cyanide; With tert-butylmagnesium chloride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/ol0498592

Reference yield: 89.0%

: 1068-55-9
isopropylmagnesium chloride

: 680997-58-4
carbonic acid 2-bromo-3-tert-butoxycarbonyloxy-6-formyl-phenyl ester tert-butyl ester

: 680997-59-5
carbonic acid 2-bromo-3-hydroxy-4-(3-methyl-butyl)-phenyl ester tert-butyl ester

Guidance literature:: carbonic acid 2-bromo-3-tert-butoxycarbonyloxy-6-formyl-phenyl ester tert-butyl ester; With sodium tetrahydroborate; In tetrahydrofuran; water; at 0 ℃; for 0.00333333h;

isopropylmagnesium chloride; In diethyl ether; at -78 - 20 ℃; for 4.16667h;
DOI:10.1021/ol0498592