(1R)-1-(4,5-diphenyloxazol-2-yl)methylamino-5-ethoxycarbonylmethoxy-1,2,3,4-tetrahydronaphthalene

Base Information

Chemical Name:(1R)-1-(4,5-diphenyloxazol-2-yl)methylamino-5-ethoxycarbonylmethoxy-1,2,3,4-tetrahydronaphthalene
CAS No.:187991-93-1
Molecular Formula:C₃₀H₃₀N₂O₄
Molecular Weight:482.579
Hs Code.:

Synonyms:(1R)-1-(4,5-diphenyloxazol-2-yl)methylamino-5-ethoxycarbonylmethoxy-1,2,3,4-tetrahydronaphthalene

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Chemical Property of (1R)-1-(4,5-diphenyloxazol-2-yl)methylamino-5-ethoxycarbonylmethoxy-1,2,3,4-tetrahydronaphthalene

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Technology Process of (1R)-1-(4,5-diphenyloxazol-2-yl)methylamino-5-ethoxycarbonylmethoxy-1,2,3,4-tetrahydronaphthalene

There total 6 articles about (1R)-1-(4,5-diphenyloxazol-2-yl)methylamino-5-ethoxycarbonylmethoxy-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (1R)-1-(4,5-diphenyloxazol-2-yl)methylamino-5-t-butyldiphenylsilyloxy-1,2,3,4-tetrahydronaphthalene

: 105-36-2
ethyl bromoacetate

: 187991-93-1
(1R)-1-(4,5-diphenyloxazol-2-yl)methylamino-5-ethoxycarbonylmethoxy-1,2,3,4-tetrahydronaphthalene

Guidance literature:: With NaH; tetrabutyl ammonium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 5-(tert-butyl-diphenyl-silanyloxy)-1,2,3,4-tetrahydro-naphthalen-1-ylamine

: 187991-93-1
(1R)-1-(4,5-diphenyloxazol-2-yl)methylamino-5-ethoxycarbonylmethoxy-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / K₂CO₃ / dimethylformamide

2: Bu₄NF / tetrahydrofuran

3: K₂CO₃ / dimethylformamide

With tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2005.04.042

Reference yield:

: 187993-41-5
(1R)-1-(4,5-diphenyloxazol-2-yl)methylamino-5-t-butyldiphenylsilyloxy-1,2,3,4-tetrahydronaphthalene

: 187991-93-1
(1R)-1-(4,5-diphenyloxazol-2-yl)methylamino-5-ethoxycarbonylmethoxy-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: Bu₄NF / tetrahydrofuran

2: K₂CO₃ / dimethylformamide

With tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2005.04.042