(2S,3S)-3-benzyloxy-6-hydroxy-1-triphenylmethoxy-2-hexyl methanesulfonate

Base Information

Chemical Name:(2S,3S)-3-benzyloxy-6-hydroxy-1-triphenylmethoxy-2-hexyl methanesulfonate
CAS No.:115793-29-8
Molecular Formula:C₃₃H₃₆O₆S
Molecular Weight:560.711
Hs Code.:

Synonyms:(2S,3S)-3-benzyloxy-6-hydroxy-1-triphenylmethoxy-2-hexyl methanesulfonate

Suppliers and Price of (2S,3S)-3-benzyloxy-6-hydroxy-1-triphenylmethoxy-2-hexyl methanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-3-benzyloxy-6-hydroxy-1-triphenylmethoxy-2-hexyl methanesulfonate

Chemical Property:

Purity/Quality:

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Technology Process of (2S,3S)-3-benzyloxy-6-hydroxy-1-triphenylmethoxy-2-hexyl methanesulfonate

There total 12 articles about (2S,3S)-3-benzyloxy-6-hydroxy-1-triphenylmethoxy-2-hexyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115793-28-7
(2S,3S)-3-benzyloxy-6-(tert-butyldiphenylsiloxy)-1-triphenylmethoxyhexan-2-ol

: 115793-29-8
(2S,3S)-3-benzyloxy-6-hydroxy-1-triphenylmethoxy-2-hexyl methanesulfonate

: 115690-07-8
(2R,3R)-3-benzyloxy-6-hydroxy-1-triphenylmethoxy-2-hexyl methanesulfonate

Guidance literature:

Reference yield:

: 115690-08-9
Methanesulfonic acid (1S,2S)-2-benzyloxy-5-(tert-butyl-diphenyl-silanyloxy)-1-trityloxymethyl-pentyl ester

: 115793-29-8
(2S,3S)-3-benzyloxy-6-hydroxy-1-triphenylmethoxy-2-hexyl methanesulfonate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 14h; Yield given; Ambient temperature;
DOI:10.1248/cpb.37.2391

Reference yield:

: 76-83-5
trityl chloride

: 115793-29-8
(2S,3S)-3-benzyloxy-6-hydroxy-1-triphenylmethoxy-2-hexyl methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / Et₃N / toluene / 3 h / Heating

2: 39.42 g / Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

3: Bu₄NF / tetrahydrofuran / 14 h / Ambient temperature

With tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1248/cpb.37.2391